3-(4-氯苯基)-吡啶合成路线 （共 10 条）
反应条件
potassium acetate; bis(dibenzylideneacetone)-palladium(0); tri-cyclo-hexyl-phosphine in 1,4-dioxane T=80°C; 72 h; Inert atmosphere;
参考文献
Su, Shi-Jian; Tanaka, Daisaku; Li, Yan-Jun; Sasabe, Hisahiro; Takeda, Takashi; Kido, Junji
Organic Letters, 2008 , vol. 10, # 5 p. 941 - 944
反应条件
[Pd(η3-1-Ph-allyl)(μ-Cl)]2; (Mor-DalPhos); ammonia; sodium t-butanolate in 1,4-dioxane T=110°C; 1 h; Inert atmosphere; chemoselective reaction;
参考文献
Lundgren, Rylan J.; Peters, Brendan D.; Alsabeh, Pamela G.; Stradiotto, Mark
Angewandte Chemie - International Edition, 2010 , vol. 49, # 24 p. 4071 - 4074
反应条件
potassium carbonate in isopropyl alcohol
T=85 - 90°C; Suzuki-Miyaura Coupling; 24 h;
参考文献
Santra, Subhankar; Hota, Pradip Kumar; Bhattacharyya, Rangeet; Bera, Parthasarathi; Ghosh, Prasenjit; Mandal, Swadhin K.
ACS Catalysis, 2013 , vol. 3, # 12 p. 2776 - 2789
反应条件
palladium diacetate; potassium carbonate in dimethyl sulfoxide
T=60°C; Suzuki Coupling; Inert atmosphere;
参考文献
Liu, Jin-Biao; Yan, Hui; Chen, Hui-Xuan; Luo, Yu; Weng, Jiang; Lu, Gui
Chemical Communications, 2013 , vol. 49, # 46 p. 5268 - 5270
反应条件
potassium hydroxide; tetrakis(triphenylphosphine) palladium(0); tetrabutylammomium bromide in tetrahydrofuran
2 h; Heating;
参考文献
Ishikura, Minoru; Kamada, Machiko; Terashima, Masanao
Heterocycles, 1984 , vol. 22, # 2 p. 265 - 268
反应条件
K3PO4*3H2O in tetrahydrofuran; water
Suzuki coupling; 6 h; Reflux;
参考文献
Kumar, V. K. Ratheesh; Krishnakumar, Sreedevi; Gopidas, Karical R.
European Journal of Organic Chemistry, 2012 , # 18 p. 3447 - 3458
反应条件
potassium acetate; 18-crown-6 ether
1.5 h; Ambient temperature; Yield given. Yields of byproduct given;
参考文献
Beadle, James R.; Korzeniowsky, Stephen H.; Rosenberg, David E.; Garcia-Slanga, Blanche J.; Gokel, George W.
Journal of Organic Chemistry, 1984 , vol. 49, # 9 p. 1594 - 1603
反应条件
tricyclohexylphosphine-Au(I); potassium tert-butylate
T=60°C; 24 h; Inert atmosphere;
参考文献
Li, Ming; Hua, Ruimao
Tetrahedron Letters, 2009 , vol. 50, # 13 p. 1478 - 1481
反应条件
1,10-phenanthroline; palladium diacetate; caesium carbonate
T=140°C; 48 h; Sealed tube;
参考文献
Ye, Mengchun; Gao, Guo-Lin; Edmunds, Andrew J. F.; Worthington; Morris, James A.; Yu, Jin-Quan
Journal of the American Chemical Society, 2011 , vol. 133, # 47 p. 19090 - 19093
反应条件
1 h; Ambient temperatureIrradiation; Title compound not separated from byproducts;
参考文献
Ohkura, Kazue; Seki, Koh-ichi; Terashima, Masanao; Kanaoka, Yuichi
Tetrahedron Letters, 1989 , vol. 30, # 26 p. 3433 - 3436
