1: phenyl-magnesium bromide With ZnI2(tmeda) in tetrahydrofuran
2: (4'-Oxapentan-2'-yl) toluene-p-sulfonate With anhydrous iron chloride in tetrahydrofuran
T=0 - 40°C;
hydrogen; palladium in methanol
T=20°C; P=760 Torr; effects of solvent and catalyst on hydrogenation of title compound; Rate constantProduct distribution;
参考文献
Cerveny, Libor; Sabata, Stanislav; Ruzicka, Vlastimil
Collection of Czechoslovak Chemical Communications, 1980 , vol. 45, # 12 p. 3525 - 3531