乙基(2E)-3-(3-吡啶基)丙烯酸酯合成路线 （共 37 条）
反应条件
zinc; tris-(dimethylamino)-phosphine in toluene T=110°C; 18 h;
参考文献
Khan, R H; Rastogi, R C
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1992 , vol. 31, # 4 p. 276
反应条件
sodium in ethanol T=-15 - -5°C; 2 h;
参考文献
Journal of Organic Chemistry, , vol. 56, # 5 p. 1922 - 1927
反应条件
tributylphosphine; tetrakis(triphenylphosphine) palladium(0) in benzene T=80°C; 24 h; Yield given. Yields of byproduct given;
参考文献
Tetrahedron Letters, , vol. 32, # 4 p. 513 - 514
反应条件
tert.-butylnitrite; chloroacetic acid; bis(dibenzylideneacetone)-palladium(0) in dichloromethane 0.5 h; Ambient temperature;
参考文献
Kikukawa, Kiyoshi; Maemura, Koji; Kiseki, Yasuyuki; Wada, Fumio; Matsuda, Tsutomu; Giam, Choo S.
Journal of Organic Chemistry, 1981 , vol. 46, # 24 p. 4885 - 4888
反应条件
caesium carbonate in acetonitrile 1 h; Heating;
参考文献
Lee, Jong Chan; Oh, Yoon Seok; Cho, Sung Hye; Lee, Jung Il
Organic Preparations and Procedures International, 1996 , vol. 28, # 4 p. 480 - 483
反应条件
hydrogenchloride 24 h; Heating;
参考文献
Rico, Joseph G.; Lindmark, Richard J.; Fogers, Thomas E.; Bovy, Philippe R.
Journal of Organic Chemistry, 1993 , vol. 58, # 27 p. 7948 - 7951
反应条件
1.1: n-butyllithium / tetrahydrofuran; hexane / 0.17 h / -100 °C 1.2: 91 percent / tetrahydrofuran; hexane / 2 h / -100 - 0 °C 2.1: 85 percent / PPh3; Et3N; Pd(OAc)2 / dimethylformamide / 16 h / 130 °C 3.1: 85 percent / tetrabutylammonium fluoride / tetrahydrofuran / 16 h / 20 °C View Scheme
参考文献
Organic Letters, , vol. 7, # 3 p. 363 - 366
反应条件
1: 85 percent / PPh3; Et3N; Pd(OAc)2 / dimethylformamide / 16 h / 130 °C 2: 85 percent / tetrabutylammonium fluoride / tetrahydrofuran / 16 h / 20 °C View Scheme
参考文献
Organic Letters, , vol. 7, # 3 p. 363 - 366
反应条件
oxygen in toluene T=110°C; one-pot alcohol oxidation-Wittig reaction; 24 h;
参考文献
European Journal of Organic Chemistry, , # 18 p. 2943 - 2946
反应条件
hollandite in toluene T=110°C; Wittig Olefination; 4 h; Catalytic behavior; diastereoselective reaction;
参考文献
Kona, Jagadeswara R.; King'Ondu, Cecil K.; Howell, Amy R.; Suib, Steven L.
ChemCatChem, 2014 , vol. 6, # 3 p. 749 - 752
