1-(1-羟基环己基)-3,3-二甲基-2-丁酮合成路线 （共 6 条）
反应条件
[2,2']bipyridinyl; tetra-n-butylammonium tetrafluoroborate; ethylene dibromide in N,N-dimethyl-formamide
T=20°C; Electrolysisnickel sponge cathode; iron sacrificial rod anode;
参考文献
Durandetti, Muriel; Meignein, Clothilde; Perichon, Jacques
Organic Letters, 2003 , vol. 5, # 3 p. 317 - 320
参考文献
Curran, Dennis P.; Scanga, Susan A.; Fenk, Christopher J.
Journal of Organic Chemistry, 1984 , vol. 49, # 19 p. 3474 - 3478
反应条件
(i) nBuLi, iPr2NH, hexane, Et2O, (ii) /BRN= 385735/; Multistep reaction;
参考文献
House,H.O.; Snoble,K.A.J.
Journal of Organic Chemistry, 1976 , vol. 41, # 19 p. 3076 - 3083
反应条件
toluene-4-sulfonic acid in benzene
Heating;
参考文献
House,H.O.; Snoble,K.A.J.
Journal of Organic Chemistry, 1976 , vol. 41, # 19 p. 3076 - 3083
反应条件
phosphorus trichoride in benzene
1.5 h; Heating; Yield given. Title compound not separated from byproducts;
参考文献
Sosnovskikh, V. Ya.; Esafov, V. I.; Andreev, N. S.
Journal of Organic Chemistry USSR (English Translation), 1981 , vol. 17, # 11 p. 2096 - 2100
Zhurnal Organicheskoi Khimii, 1981 , vol. 17, # 11 p. 2346 - 2350
反应条件
disodium hydrogenphosphate; CF3CO3H in dichloromethane
1 h; Heating;
参考文献
Curran, Dennis P.; Scanga, Susan A.; Fenk, Christopher J.
Journal of Organic Chemistry, 1984 , vol. 49, # 19 p. 3474 - 3478
