1-氯-4-环己基硫基苯合成路线 （共 10 条）
反应条件
N,N,N',N',N'',N''-hexamethylphosphoric triamide; ethylmagnesium bromide in tetrahydrofuran
T=20°C; 0.133333 h;
参考文献
Satoh, Tsuyoshi; Akita, Kiyoshi
Chemical and pharmaceutical bulletin, 2003 , vol. 51, # 2 p. 181 - 186
反应条件
pyridine; copper diacetate; 4 A molecular sieve in N,N-dimethyl-formamide
Substitution; 5 h; Heating;
参考文献
Herradura, Prudencio S.; Pendola, Kathleen A.; Guy, R. Kiplin
Organic Letters, 2000 , vol. 2, # 14 p. 2019 - 2022
反应条件
tert.-butylhydroperoxide
T=120°C; 18 h; Sealed tubeInert atmosphere;
参考文献
Du, Bingnan; Jin, Bo; Sun, Peipei
Organic Letters, 2014 , vol. 16, # 11 p. 3032 - 3035
反应条件
water
T=20°C; anti-Markovnikov addition; 2.5 h;
参考文献
Ranu, Brindaban C.; Mandal, Tanmay
Synlett, 2007 , # 6 p. 925 - 928
反应条件
1: aq. NaHCO3; MCPBA / CHCl3 / 0 °C
2: 93 percent / EtMgBr; HMPA / tetrahydrofuran / 0.13 h / 20 °C
View Scheme
参考文献
Satoh, Tsuyoshi; Akita, Kiyoshi
Chemical and pharmaceutical bulletin, 2003 , vol. 51, # 2 p. 181 - 186
反应条件
1: BF3*Et2O / CHCl3 / 0 °C
2: aq. NaHCO3; MCPBA / CHCl3 / 0 °C
3: 93 percent / EtMgBr; HMPA / tetrahydrofuran / 0.13 h / 20 °C
View Scheme
参考文献
Satoh, Tsuyoshi; Akita, Kiyoshi
Chemical and pharmaceutical bulletin, 2003 , vol. 51, # 2 p. 181 - 186
反应条件
aluminium trichloride
24 h; Ambient temperature; Further byproducts given;
参考文献
El-Zohry, Maher F.
Phosphorus, Sulfur and Silicon and the Related Elements, 1992 , vol. 66, # 14 p. 311 - 320
反应条件
1: carbon disulfide; S2cl2
View Scheme
参考文献
Bloomfield
Journal of the Chemical Society, 1947 , p. 1549
参考文献
Bloomfield
Journal of the Chemical Society, 1947 , p. 1549
参考文献
Bloomfield
Journal of the Chemical Society, 1947 , p. 1549
