2,2-二甲基-3-氧代丁酸乙酯合成路线 (共 56 条)
参考文献
Schryver
Journal of the Chemical Society, 1893 , vol. 63, p. 1336
反应条件
potassium-sodium in diethyl ether
参考文献
le Goaller,R.; Dierre,J.-L.
Canadian Journal of Chemistry, 1977 , vol. 55, p. 757 - 765
参考文献
Adickes et al.
Journal fuer Praktische Chemie (Leipzig), 1932 , vol. <2>133, p. 313
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Hauser; Hudson
Journal of the American Chemical Society, 1940 , vol. 62, p. 65
反应条件
phosphorus pentachloride nachfolgendes Verseifen des entstehenden Aethylesters mit alkoh. Kalilauge;
参考文献
Wash, Paul L.; Maverick, Emily; Chiefari, John; Lightner, David A.
Journal of the American Chemical Society, 1997 , vol. 119, # 16 p. 3802 - 3806
反应条件
1: PCl5 2: NaOH 3: 80 percent / NaNH2 View Scheme
参考文献
Wash, Paul L.; Maverick, Emily; Chiefari, John; Lightner, David A.
Journal of the American Chemical Society, 1997 , vol. 119, # 16 p. 3802 - 3806
反应条件
bis-(2-hydroxy-ethyl)-amine; B-chloro-diisopinocampheylborane 1) neat, room t., 12 days h; 2) ethyl ether, 2 h; Yield given. Multistep reaction. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Brown, Herbert C.; Chandrasekharan, J.; Ramachandran, P. V.
Journal of the American Chemical Society, 1988 , vol. 110, # 5 p. 1539 - 1546
参考文献
Dieckmann
Chemische Berichte, 1900 , vol. 33, p. 2683
Justus Liebigs Annalen der Chemie, 1901 , vol. 317, p. 108
参考文献
Keay; Rodrigo
Journal of the American Chemical Society, 1982 , vol. 104, # 17 p. 4725 - 4727
反应条件
tri-n-butylborane in benzene Irradiation;
参考文献
Utimoto,K. et al.
Tetrahedron Letters, 1972 , p. 1167 - 1168
反应条件
1: concentrated aq. barium hydroxide solution 2: sodium amide; diethyl ether / nachfolgenden Einleiten von Acetylen unter Druck View Scheme
参考文献
Leers
Bulletin de la Societe Chimique de France, 1926 , vol. <4>39, p. 423