in not given dropwise addn. of thionyl chloride to tetraalkyltin(IV) compd. under dry N2 atmosphere under ice cooling, warming to room temp., refluxing for 30 min; distn. (removal of excess of SOCl2), cooling resulting liquids, sepn., elem. anal.;
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C.A., 1948 , p. 6742
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Gmelin Handbook: Sn: Org.Verb.1, 1.1.1.2.4.8, page 76 - 79
tetrachloromethane byproducts: C2H6, C2H4; Irradiation (UV/VIS); for 8 h;
参考文献
Cahours, A.
Liebigs Annalen der Chemie, 1862 , vol. 122, p. 48 - 71
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Frankland, E.
Liebigs Annalen der Chemie, 1859 , vol. 111, p. 44 - 68
Nash, G. A.; Skinner, H. A.; Stack, W. F.
Transactions of the Faraday Society, 1965 , vol. 61, p. 640 - 648
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Gmelin Handbook: Sn: Org.Verb.1, 1.1.1.2.4.8, page 76 - 79
Goddard, D.; Goddard, A. E.
Journal of the Chemical Society, 1922 , vol. 121, p. 256 - 261
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Gmelin Handbook: Sn: Org.Verb.1, 1.1.1.2.4.8, page 76 - 79
