4'-戊基-[1,1'-联苯]-4-甲酰氯合成路线 （共 7 条）
参考文献
Merck Patent Gesellschaft mit beschrankter Haftung
Patent: US4065489 A1, 1977 ;
反应条件
oxalyl dichloride in benzene
0.5 h;
参考文献
Solladie, Guy; Zimmermann, Richard
Journal of Organic Chemistry, 1985 , vol. 50, # 21 p. 4062 - 4068
反应条件
1: 66 percent / KOH / bis-(2-hydroxy-ethyl) ether / 12 h / 100 °C
2: 79 percent / SOCl2; DMF / Heating
View Scheme
参考文献
Griesar; Soto-Bustamante; Haase
Zeitschrift fur Naturforschung - Section B Journal of Chemical Sciences, 2000 , vol. 55, # 7 p. 567 - 575
反应条件
in pyridine; toluene
3 h; Heating;
参考文献
Hong, X. J.; Ge, M. J.; Zhao, X. M.; Fen, Z. R.; Liu, Z. J.
Molecular Crystals and Liquid Crystals (1969-1991), 1983 , vol. 99, p. 81 - 88
反应条件
in pyridine; toluene
3 h; Heating;
参考文献
Hong, X. J.; Ge, M. J.; Zhao, X. M.; Fen, Z. R.; Liu, Z. J.
Molecular Crystals and Liquid Crystals (1969-1991), 1983 , vol. 99, p. 81 - 88
反应条件
in pyridine; toluene
3 h; Heating;
参考文献
Hong, X. J.; Ge, M. J.; Zhao, X. M.; Fen, Z. R.; Liu, Z. J.
Molecular Crystals and Liquid Crystals (1969-1991), 1983 , vol. 99, p. 81 - 88
反应条件
pyridine in diethyl ether
6 h;
参考文献
Bezborodov, V. S.; Lapanik, V. I.
Journal of Organic Chemistry USSR (English Translation), 1990 , vol. 26, # 10.2 p. 1880 - 1882
Zhurnal Organicheskoi Khimii, 1990 , vol. 26, # 10 p. 2178 - 2181
