N-对甲苯基-对甲苯磺胺合成路线 （共 64 条）
反应条件
1: NaOH-solution 2: sulfuric acid / 120 °C View Scheme
参考文献
Halberkann
Chemische Berichte, 1921 , vol. 54, p. 1837
参考文献
Clemo; Perkin
Journal of the Chemical Society, 1925 , vol. 127, p. 2303
反应条件
perchloric acid; acetic acid 1 h; Heating;
参考文献
Kudav, D.P.; Samant,S.P.; Hosangadi, B.D.
Synthetic Communications, 1987 , vol. 17, # 10 p. 1185 - 1188
参考文献
Witt; Uermenyi
Chemische Berichte, 1913 , vol. 46, p. 303
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Halberkann
Chemische Berichte, 1921 , vol. 54, p. 1837
反应条件
1,10-phenanthroline; palladium (II) trifluoroacetate; oxygen in toluene
T=140°C; 40 h;
参考文献
Cao, Xiangxiang; Bai, Yang; Xie, Yanjun; Deng, Guo-Jun
Journal of Molecular Catalysis A: Chemical, 2014 , vol. 383-384, p. 94 - 100
反应条件
potassium carbonate in water
1.5 h; RefluxGreen chemistry;
参考文献
Nasrollahzadeh, Mahmoud; Rostami-Vartooni, Akbar; Ehsani, Ali; Moghadam, Majid
Journal of Molecular Catalysis A: Chemical, 2014 , vol. 387, p. 123 - 129
反应条件
CuI; potassium carbonate in N,N-dimethyl-formamide
参考文献
Buchwald, Stephen L.; Klapars, Artis; Antilla, Jon C.; Job, Gabriel E.; Wolter, Martina; Kwong, Fuk Y.; Nordmann, Gero; Hennessy, Edward J.
Patent: US2003/65187 A1, 2003 ;
反应条件
copper(l) chloride in methanol
T=20°C; Chan-Lam Coupling; 0.5 h;
参考文献
Moon, Soo-Yeon; Nam, Jungsoo; Rathwell, Kris; Kim, Won-Suk
Organic Letters, 2014 , vol. 16, # 2 p. 338 - 341
反应条件
pyridine in dichloromethane
T=20°C; 16 h;
参考文献
Alp, Cemalettin; Oezsoy, Seyda; Alp, Nurdan Alcan; Erdem, Deryanur; Gueltekin, Mehmet Serdar; Kuefrevioglu, Oemer Irfan; Sentuerk, Murat; Supuran, Claudiu T.
Journal of Enzyme Inhibition and Medicinal Chemistry, 2012 , vol. 27, # 6 p. 818 - 824
反应条件
ammonium hydroxide; iron in methanol
T=25°C; Reduction; condensation; 1 h; sonication;
参考文献
Chandrasekhar; Narsihmulu
Tetrahedron Letters, 2000 , vol. 41, # 41 p. 7969 - 7972
