2,4-二甲基-3-戊醇合成路线 (共 83 条)
参考文献
Bulletin des Societes Chimiques Belges, , vol. 35, p. 382
Chem. Zentralbl., , vol. 98, # I p. 715
参考文献
Bulletin des Societes Chimiques Belges, , vol. 35, p. 382
Chem. Zentralbl., , vol. 98, # I p. 715
反应条件
potassium hydroxide; Ru(CF3CO2)CO(PPh3)2 T=140°C; 200 h; Equilibrium constant;
参考文献
Graser, Barbara; Strohmeier, Walter; Marcec, Radovan; Steigerwald, Hannelore
Berichte der Bunsen-Gesellschaft, 1981 , vol. 85, # 7 p. 671 - 677
反应条件
trichloroacetonitrile; triphenylphosphine in acetonitrile T=-15 - 20°C;
参考文献
Graf, Claus-Dieter; Malan, Christophe; Harms, Klaus; Knochel, Paul
Journal of Organic Chemistry, 1999 , vol. 64, # 15 p. 5581 - 5588
反应条件
trichloroacetonitrile; triphenylphosphine in 1,2-dichloro-benzene T=-7°C; 24 h; other alcohols; other halogenating agents; also with use of iodide and thiocyanate ions; var. solvents, temp. and reaction times; Product distribution;
参考文献
Matveeva, E. D.; Yalovskaya, A. I.; Cherepanov, I. A.; Bundel', Yu. G.; Kurts, A. L.
Journal of Organic Chemistry USSR (English Translation), 1991 , vol. 27, # 8.1 p. 1409 - 1415
Zhurnal Organicheskoi Khimii, 1991 , vol. 27, # 8 p. 1611 - 1618
反应条件
T=128 - 158°C; Thermolysis; Kinetics;
参考文献
Kharasch et al.
Journal of Organic Chemistry, 1951 , vol. 16, p. 113,125
反应条件
copper(II) bis(trifluoromethanesulfonate)
参考文献
Laali, Khosrow; Gerzina, Robert J.; Flajnik, Christine M.; Geric, Cynthia M.; Dombroski, Ann Marie
Helvetica Chimica Acta, 1987 , vol. 70, p. 607 - 611
反应条件
aluminum oxide T=350 - 375°C;
参考文献
Henne; Matuszak
Journal of the American Chemical Society, 1944 , vol. 66, p. 1651
Full Text Show Details
Goldwasser; Taylor
Journal of the American Chemical Society, 1939 , vol. 61, p. 1757
反应条件
trichloroacetonitrile; triphenylphosphine in 1,2-dichloro-benzene T=-7°C; 24 h; other alcohols; other halogenating agents; also with use of iodide and thiocyanate ions; var. solvents, temp. and reaction times; Product distribution;
参考文献
Matveeva, E. D.; Yalovskaya, A. I.; Cherepanov, I. A.; Bundel', Yu. G.; Kurts, A. L.
Journal of Organic Chemistry USSR (English Translation), 1991 , vol. 27, # 8.1 p. 1409 - 1415
Zhurnal Organicheskoi Khimii, 1991 , vol. 27, # 8 p. 1611 - 1618
反应条件
T=398°C; bei raschem Ueberleiten;
参考文献
Henne; Matuszak
Journal of the American Chemical Society, 1944 , vol. 66, p. 1651
Full Text Show Details
Goldwasser; Taylor
Journal of the American Chemical Society, 1939 , vol. 61, p. 1757