1-环己基-2-羟基-乙酮合成路线 （共 28 条）
反应条件
oxygen; lt;Bi(III)(mandelate)2gt;2(μ-O) in dimethyl sulfoxide T=80°C; 4 h;
参考文献
Tetrahedron, , vol. 51, # 17 p. 4991 - 4996
反应条件
1,3-bis(2,4,6-trimethylphenyl)imidazolinium-2-carboxylate in tetrahydrofuran
T=60°C; 20 - 44 h; Product distribution / selectivity;
参考文献
Degussa GmbH
Patent: US2008/51608 A1, 2008 ;
Location in patent: Page/Page column 6; 10 ;
反应条件
1: With ozone in dichloromethane
T=-78°C;
2: With triphenylphosphine in dichloromethane
3: With 1,8-diazabicyclo[5.4.0]undec-7-ene in dichloromethane
T=-78 - 20°C; 8 h;
参考文献
Hon, Yung-Son; Wong, Ying-Chieh; Wu, Kuo-Jui
Journal of the Chinese Chemical Society, 2008 , vol. 55, # 4 p. 896 - 914
反应条件
1,4-dioxane; sulfuric acid
参考文献
Linnell; Roushdi
Quarterly Journal of Pharmacy and Pharmacology, 1939 , vol. 12, p. 252,254, 258
反应条件
potassium hydroxide; formic acid ethyl ester in ethanol
4 h; Heating;
参考文献
Ogawa; Terada; Muranaka; Hamakawa; Fujii
Chemical and Pharmaceutical Bulletin, 1987 , vol. 35, # 6 p. 2426 - 2436
反应条件
4-methylmorpholine N-oxide; lithium diisopropyl amide; osmium(VIII) oxide
1.) THFC, 2.) aq. acetone, -5 to 25 deg C, 9 h; Yield given. Multistep reaction;
参考文献
McCormick, J. P.; Tomasik, Witold; Johnson, Mark W.
Tetrahedron Letters, 1981 , vol. 22, p. 607 - 610
反应条件
N(Et)4ClO4 in N,N-dimethyl-formamide
T=20°C; mercury pool electrode;
参考文献
Chiarotto, Isabella; Feroci, Marta; Giomini, Claudio; Inesi, Achille
Bulletin de la Societe Chimique de France, 1996 , vol. 133, # 2 p. 167 - 175
反应条件
diethyl ether; sodium methylate
anschliessendes Behandeln mit H2O;
参考文献
Wagner; Moore
Journal of the American Chemical Society, 1950 , vol. 72, p. 2884,2886
反应条件
aluminum oxide; sodium bromite
Ambient temperature;
参考文献
Morimoto, Takashi; Hirano, Masao; Iwasaki, Keiko; Ishikawa, Takashi
Chemistry Letters, 1994 , # 1 p. 53 - 54
反应条件
2: water; HBr
3: sodium methylate; diethyl ether / anschliessendes Behandeln mit H2O
View Scheme
参考文献
Wagner; Moore
Journal of the American Chemical Society, 1950 , vol. 72, p. 2884,2886
