1,1'-联-2-萘酚合成路线 (共 233 条)
反应条件
4-(N,N-dimethlyamino)pyridine in isopropyl alcohol T=20°C;
参考文献
Schafer, Wes A.; Hobbs, Steve; Rehm, Jason; Rakestraw, David A.; Orella, Charles; McLaughlin, Mark; Ge, Zhihong; Welch, Christopher J.
Organic Process Research and Development, 2007 , vol. 11, # 5 p. 870 - 876
反应条件
phosphoric acid; trifluoroacetic anhydride in water T=50°C; 0.25 h;
参考文献
Costantino, Andrea R.; Ocampo, Romina A.; Schneider, Maria G. Montiel; Fernandez, Gustavo; Koll, Liliana C.; Mandolesi, Sandra D.
Synthetic Communications, 2013 , vol. 43, # 23 p. 3192 - 3202
反应条件
1.1: 95 percent / pyridine / toluene / 3.5 h / 0 - 25 °C 2.1: Mg / tetrahydrofuran / Heating 2.2: 80 percent / NiCl2(dppp) / tetrahydrofuran / 0.5 h / Heating View Scheme
参考文献
Ooi, Takashi; Kameda, Minoru; Maruoka, Keiji
Journal of the American Chemical Society, 1999 , vol. 121, # 27 p. 6519 - 6520
反应条件
sodium hydroxide in ethanol Reflux;
参考文献
Kertmen, Ahmet; Szczygelska-Tao, Jolanta; Chojnacki, Jaroslaw
Tetrahedron, 2013 , vol. 69, # 49 p. 10662 - 10668
反应条件
1: 1.) NaH / 1.) DMF, 70 deg C, 1 h, 2.) DMF, 70 deg C, 48 h 2: conc. HCl / methanol / 1 h / Ambient temperature View Scheme
参考文献
Yan, Yuan-Yong; Widhalm, Michael
Tetrahedron Asymmetry, 1998 , vol. 9, # 20 p. 3607 - 3610
反应条件
N-ethyl-N,N-diisopropylamine in dichloromethane T=5°C; 1 h;
参考文献
Takata, Toshikazu; Matsuoka, Hideo; Endo, Takeshi
Chemistry Letters, 1991 , # 12 p. 2091 - 2094
参考文献
Journal of the American Chemical Society, , vol. 102, # 27 p. 7932 - 7934
反应条件
bromine; triphenylphosphine in acetonitrile T=230 - 300°C;
参考文献
Tetrahedron, , vol. 60, # 20 p. 4387 - 4397
反应条件
bromine in acetonitrile microwave irradiation;
参考文献
Synthetic Communications, , vol. 33, # 16 p. 2763 - 2767
反应条件
acetonitrile, 60 deg C, 30 min then 260-270 deg C, 1 h then 311-320 deg C, 1 h; Yield given;
参考文献
Tetrahedron, , vol. 40, # 8 p. 1245 - 1253