1,1'-联-2-萘酚合成路线 （共 233 条）
反应条件
in toluene Substitution; Heating;
参考文献
Ma, Margaret F. P.; Li, Kangying; Zhou, Zhenghong; Tang, Chuchi; Chan, Albert S. C.
Tetrahedron Asymmetry, 1999 , vol. 10, # 17 p. 3259 - 3261
反应条件
1: 45 percent / (C6H5)3PBr2 / 320 °C 2: 78 percent / t-C4H9Li / tetrahydrofuran View Scheme
参考文献
Journal of the American Chemical Society, , vol. 102, # 27 p. 7932 - 7934
反应条件
1: With copper(l) chloride; (+)-sparteine surrogate in methanol; dichloromethane T=-20 - 20°C; 24 h; Inert atmosphereDarkness; 2: With sodium hydrogencarbonate in methanol; dichloromethane; water T=-20°C; optical yield given as percent eeenantioselective reaction;
参考文献
Hu, Gang; Holmes, Daniel; Gendhar, Brina Fay; Wulff, William D.
Journal of the American Chemical Society, 2009 , vol. 131, # 40 p. 14355 - 14364
反应条件
1: With copper(l) chloride; (+)-sparteine surrogate in methanol; dichloromethane T=25°C; 24 h; Inert atmosphereDarkness; 2: With sodium hydrogencarbonate in methanol; dichloromethane; water optical yield given as percent eeenantioselective reaction;
参考文献
Journal of the American Chemical Society, , vol. 131, # 40 p. 14355 - 14364
反应条件
in acetonitrile 3 h; Reflux;
参考文献
Tetrahedron: Asymmetry, , vol. 23, # 18-19 p. 1327 - 1331,5
反应条件
(8S,9R)-(-)-N-benzyl-cinchonidinium chloride in acetonitrile resolution of racemate; 4 h; Heating;
参考文献
Journal of Organic Chemistry, , vol. 65, # 20 p. 6319 - 6337
反应条件
Pseudomonas sp. lipoprotein lipase in isopropyl alcohol; acetone T=40°C; 120 h;
参考文献
Juarez-Hernandez, Marcela; Johnson, Dean V.; Holland, Herbert L.; McNulty, James; Capretta, Alfredo
Tetrahedron Asymmetry, 2003 , vol. 14, # 3 p. 289 - 291
反应条件
1: in methanol T=50°C; 1 h; 2: With hydrogenchloride in water; ethyl acetate Product distribution / selectivity;
参考文献
LUPIN LIMITED; ROY, Bhairab, Nath; SINGH, Girij, Pal; LATHI, Piyush, Suresh; MITRA, Rangan
Patent: WO2011/86566 A1, 2011 ;
Location in patent: Page/Page column 32 ;
反应条件
1: in methanol T=50°C; 1 h; 2: With hydrogenchloride in water; ethyl acetate Product distribution / selectivity;
参考文献
LUPIN LIMITED; ROY, Bhairab, Nath; SINGH, Girij, Pal; LATHI, Piyush, Suresh; MITRA, Rangan
Patent: WO2011/86566 A1, 2011 ;
Location in patent: Page/Page column 32-33 ;
反应条件
C42H60N6O7 in toluene T=0°C; 24 h;
参考文献
Mueller, Christian E.; Zell, Daniela; Hrdina, Radim; Wende, Raffael C.; Wanka, Lukas; Schuler, Soeren M. M.; Schreiner, Peter R.
Journal of Organic Chemistry, 2013 , vol. 78, # 17 p. 8465 - 8484
