in tert-butyl alcohol byproducts: CO2; Heating at 120°C for 1 h in an autoclave.; GC, evapn. of solvents.;
参考文献
Journal of General Chemistry USSR (English Translation), , vol. 56, p. 287 - 289
Zhurnal Obshchei Khimii, , vol. 56, p. 330 - 333
→
反应条件
in toluene heating (90°C, 1 h); crystn. on cooling to 0°C, crystals filtration off ad drying (Ph4Bi-compd.), crystn. on cooling to -18°C (Ph4Sb-compd.), solvent removing and residue recrystn. (ethanol) yielding BiPh3;
参考文献
Russian Chemical Bulletin, , vol. 48, # 12 p. 2325 - 2329
in diethyl ether byproducts: (C6H5)2, C6H5OH; splitting into water, distillation of ether-phase, steam distillation of remained substance and extraction with ethanol;
参考文献
Zeitschrift fuer Anorganische und Allgemeine Chemie, , vol. 115, p. 253 - 272
