in dichloromethane-d2 byproducts: (CH3)2C4H4(CH3CO)CH2COH; under N2; an equimolar mixt. of Bi-contg. compd. and (-)-pinanediol in CD2Cl2 was refluxed at room temp. for 12 h; (1)H NMR monitoring at room temp.;
参考文献
Journal of Organometallic Chemistry, , vol. 662, # 1-2 p. 98 - 104
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反应条件
in methanol-d4 byproducts: BF3, pinacol; under Ar; Bi compd. reacted with Me4NF (excess) in CD3OD;