methanol in methanol; benzene byproducts: HCl; addn. of PPh(OMe)2 to the Re compd. in benzene under inert gas flow, refluxing for 5 min, concn. (vac.), addn. of MeOH, heating and concn. at elevated temp.; addn. of Et2O, filtn., washing with Et2O, drying in vac. and recrystn. from THF-Et2O; elem. anal.;
参考文献
Carvalho, M. Fernanda N. N.; Pombeiro, Armando J. L.
Journal of Organometallic Chemistry, 1990 , vol. 384, p. 121 - 132
in tetrahydrofuran; methanol 96 h; Inert atmosphereMolecular sieveReflux;
参考文献
Li, Jie; Lutz, Martin; Spek, Anthony L.; Van Klink, Gerard P.M.; Van Koten, Gerard; Klein Gebbink, Robertus J.M.
Journal of Organometallic Chemistry, 2010 , vol. 695, # 24 p. 2618 - 2628
