aluminium trichloride in benzene benzene soln. of P4 boiled with AlCl3; orange-yellow prod. contains Al, Cl, C, H, but no P(C6H5)3;
参考文献
Boeeseken, J.
Recueil des Travaux Chimiques des Pays-Bas, 1926 , vol. 45, p. 458 - 474
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Gmelin Handbook: P: MVol.B, 3.4.2.3, page 310 - 316
methanol in ethanol; benzene byproducts: HCl; addn. of trimethylphosphite to the Re compd. in benzene under inert gas flow, refluxing for 2 h, concn. (vac.), addn. of EtOH and MeOH, heating and concn. at elevated temp.; filtn., washing with MeOH-Et2O and drying in vac.;
参考文献
Carvalho, M. Fernanda N. N.; Pombeiro, Armando J. L.
Journal of Organometallic Chemistry, 1990 , vol. 384, p. 121 - 132
