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结构式
乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
6030-60-0
合成路线
（共 10 条）
6030-60-0
→
反应条件
491-60-1
大黄素蒽酮
反应条件
1: N-bromosuccinmide; dibenzoyl peroxide / tetrachloromethane; benzene / 24 h / Reflux 2: silver nitrate / ethanol; water / Reflux 3: water; sodium hydroxide / 0.5 h / Reflux 4: hydrogenchloride; SnCl2·2H2O; acetic acid / water / 3 h / 100 °C View Scheme
参考文献
Liang, Jing Lu; Cha, Hyo Chang; Lee, Seung Ho; Son, Jong-Keun; Chang, Hyeun Wook; Eom, Ji-Eun; Kwon, Youngjoo; Jahng, Yurngdong
Archives of Pharmacal Research, 2012 , vol. 35, # 3 p. 447 - 454
6030-60-0
→
反应条件
518-82-1
大黄素
反应条件
sodium hydroxide T=80°C; 2 h;
参考文献
Hadj-Hamdri; Vidal-Cros; Gaudry; Sobrio; Rousseau
Journal of Labelled Compounds and Radiopharmaceuticals, 1995 , vol. 36, # 8 p. 795 - 799
518-82-1
大黄素
+
108-24-7
乙酸酐
→
反应条件
6030-60-0
反应条件
pyridine T=60 - 70°C; 4 h;
参考文献
Narender; Sukanya; Sharma, Komal; Bathula, Surendar Reddy
RSC Advances, 2013 , vol. 3, # 17 p. 6123 - 6131
84993-87-3
→
反应条件
6030-60-0
反应条件
hydrogen; palladium on activated charcoal in methanol 4.5 h;
参考文献
Hadj-Hamdri; Vidal-Cros; Gaudry; Sobrio; Rousseau
Journal of Labelled Compounds and Radiopharmaceuticals, 1995 , vol. 36, # 8 p. 795 - 799
518-82-1
大黄素
+
64-19-7
醋酸
→
反应条件
6030-60-0
反应条件
sulfuric acid T=70°C; 0.5 h;
参考文献
Morooka, Nobuhisa; Nakano, Sonoko; Itoi, Noriko; Ueno, Yoshio
Agricultural and Biological Chemistry, 1990 , vol. 54, # 5 p. 1247 - 1252
500357-04-0
→
反应条件
6030-60-0
反应条件
chromium; acetic acid
参考文献
Hesse
Justus Liebigs Annalen der Chemie, 1912 , vol. 388, p. 70
Justus Liebigs Annalen der Chemie, 1917 , vol. 413, p. 364
6030-60-0
→
反应条件
84993-87-3
反应条件
N-bromosuccinmide; dibenzoyl peroxide in tetrachloromethane 24 h; Heating;
参考文献
Hirose, Yoshio; Suehiro, Yoshihisa; Furukawa, Yumiko; Murakami, Takao
Chemical & Pharmaceutical Bulletin, 1982 , vol. 30, # 11 p. 4186 - 4188
6030-60-0
→
反应条件
84993-87-3
反应条件
N-bromosuccinmide; dibenzoyl peroxide in tetrachloromethane; benzene 24 h; Reflux;
参考文献
Liang, Jing Lu; Cha, Hyo Chang; Lee, Seung Ho; Son, Jong-Keun; Chang, Hyeun Wook; Eom, Ji-Eun; Kwon, Youngjoo; Jahng, Yurngdong
Archives of Pharmacal Research, 2012 , vol. 35, # 3 p. 447 - 454
6030-60-0
→
反应条件
85008-13-5
反应条件
1: 64 percent / NBS, benzoylperoxide / benzene / 24 h / Heating 2: 90 percent / NaOAc / 10 h / 90 - 100 °C View Scheme
参考文献
Rajagopalan; Seshadri
Proceedings - Indian Academy of Sciences, Section A, 1956 , vol. 44, p. 418,421
6030-60-0
→
反应条件
61350-20-7
反应条件
1: N-bromosuccinmide; dibenzoyl peroxide / tetrachloromethane; benzene / 24 h / Reflux 2: silver nitrate / ethanol; water / Reflux 3: sodium tetrahydroborate / methanol / 4 h 4: hydrogenchloride; SnCl2·2H2O; acetic acid / water / 3 h / 100 °C 5: sodium hydroxide / Reflux View Scheme
参考文献
Liang, Jing Lu; Cha, Hyo Chang; Lee, Seung Ho; Son, Jong-Keun; Chang, Hyeun Wook; Eom, Ji-Eun; Kwon, Youngjoo; Jahng, Yurngdong
Archives of Pharmacal Research, 2012 , vol. 35, # 3 p. 447 - 454
