1: With n-butyllithium in tetrahydrofuran; hexane T=-78°C; 1 h; Inert atmosphere; 2: With ammonium chloride in tetrahydrofuran; hexane; water T=-78 - 20°C; Inert atmosphere;
参考文献
Nishikawa, Yasuhiro; Yamamoto, Hisashi
Journal of the American Chemical Society, 2011 , vol. 133, # 22 p. 8432 - 8435
1: 3-buten-2-yl acetate With indium(III) chloride; dimethyl(n-butyl)amine; lithium chloride; indium; tetrakis(triphenylphosphine) palladium(0) in N,N-dimethyl-formamide T=35°C; 2: monoiodonaphthalene in N,N-dimethyl-formamide T=100°C; Title compound not separated from byproducts;
参考文献
Advanced Synthesis and Catalysis, , vol. 346, # 13-15 p. 1641 - 1645
1: (E)-crotyl acetate With indium(III) chloride; dimethyl(n-butyl)amine; lithium chloride; indium; tetrakis(triphenylphosphine) palladium(0) in N,N-dimethyl-formamide T=35°C; 2: monoiodonaphthalene in N,N-dimethyl-formamide T=100°C; Title compound not separated from byproducts;
参考文献
Advanced Synthesis and Catalysis, , vol. 346, # 13-15 p. 1641 - 1645
