α-D(+)-五乙酰葡萄糖合成路线 （共 168 条）
反应条件
indium trifluoromethanesulfonate T=0°C; 1 h; Product distribution; Further Variations:Reagentsreaction time;
参考文献
Bizier, Nicholas P.; Atkins, Shannon R.; Helland, Luke C.; Colvin, Shane F.; Twitchell, Joseph R.; Cloninger, Mary J.
Carbohydrate Research, 2008 , vol. 343, # 10-11 p. 1814 - 1818
反应条件
iodine T=80°C; 0.0833333 h;
参考文献
Mukherjee, Debaraj; Shah, Bhahwal Ali; Gupta, Pankaj; Taneja, Subhash Chandra
Journal of Organic Chemistry, 2007 , vol. 72, # 23 p. 8965 - 8968
反应条件
sulfuric acid in acetic acid T=50 - 55°C; 120 h;
参考文献
Carbohydrate Research, , vol. 219, p. 133 - 148
反应条件
sulfuric acid; acetic acid T=0 - 20°C; 72 h;
参考文献
Tetrahedron, , vol. 70, # 7 p. 1492 - 1496
反应条件
in pyridine T=0 - 20°C; Acetylation;
参考文献
Shimizu, Hiroki; Brown, Jonathan M.; Homans, Steven W.; Field, Robert A.
Tetrahedron, 1998 , vol. 54, # 32 p. 9489 - 9506
反应条件
1: 84 percent / HgO, HgBr2, CaSO4 / CHCl3 / 48 h / Ambient temperature 2: 90 percent / CH3ONa / methanol / 3 h 3: 86 percent / KOH / 130 °C 4: 93 percent / CF3COOH / CH2Cl2 / 0.5 h / 0 °C 5: oxalyl chloride, DMF / CH2Cl2 / 0.5 h 6: 52 percent / Et4NBr, molecular sieves 4A, DMF / CH2Cl2 / 72 h / Heating 7: H2 / 10percent Pd/C / acetic acid / 760 Torr 8: pyridine 9: BF3*Et2O / toluene / 6 h / 55 °C View Scheme
参考文献
Journal of Organic Chemistry, , vol. 53, # 24 p. 5629 - 5647
反应条件
boron trifluoride diethyl etherate in benzene T=20°C; 48 h;
参考文献
Sokolov; Zakharov; Studentsov
Russian Journal of General Chemistry, 2002 , vol. 72, # 5 p. 806 - 811
反应条件
perchloric acid on silica gel T=20°C; 0.5 h;
参考文献
Agnihotri, Geetanjali; Tiwari, Pallavi; Misra, Anup Kumar
Journal of Carbohydrate Chemistry, 2006 , vol. 25, # 6 p. 491 - 498
反应条件
1: NaIO4 / RuCl3*H2O; CeCl3*7H2O / H2O; ethyl acetate; acetonitrile / 0.25 h / 0 °C 2: pyridine View Scheme
参考文献
Journal of Organic Chemistry, , vol. 71, # 7 p. 2911 - 2913
反应条件
1: 52 percent / Et4NBr, molecular sieves 4A, DMF / CH2Cl2 / 72 h / Heating 2: H2 / 10percent Pd/C / acetic acid / 760 Torr 3: pyridine 4: BF3*Et2O / toluene / 6 h / 55 °C View Scheme
参考文献
Journal of Organic Chemistry, , vol. 53, # 24 p. 5629 - 5647
