2,6-二氟苯甲酰异氰酸酯合成路线 （共 32 条）
反应条件
in 1,2-dichloro-ethane Heating;
参考文献
Wang, Shuo; Allan, Robin D.; Skerritt, John H.; Kennedy, Ivan R.
Journal of Agricultural and Food Chemistry, 1998 , vol. 46, # 8 p. 3330 - 3338
参考文献
Societe Nationale des Poudres et Explosifs
Patent: US5734060 A1, 1998 ;
反应条件
tin(IV) chloride in 1,2-dichloro-benzene 2 h; Heating;
参考文献
Deng, M. Z.; Caubere, P.; Senet, J. P.; Lecolier, S.
Tetrahedron, 1988 , vol. 44, # 19 p. 6079 - 6086
反应条件
tin(IV) chloride T=90 - 145°C; 2.25 h;
参考文献
Odinokov, V. N.; Kukovinets, O. S.; Lozhkina, E. A.; Bikulova, V. Zh.; Petrova, T. D.; et al.
Bull. Russ. Acad. Sci. Div. Chem. Sci. (Engl. Transl.), 1992 , vol. 41, # 2 p. 468 - 470,374 - 376
反应条件
1: aq. NH3 View Scheme
参考文献
Bioorganic and Medicinal Chemistry Letters, , vol. 16, # 1 p. 162 - 166
反应条件
1: NH4OH 2: 81 percent / 1,2-dichloro-ethane / 24 h / Ambient temperature View Scheme
参考文献
Russian Journal of Organic Chemistry, , vol. 34, # 2 p. 202 - 204
反应条件
1: 90 percent / NaNH2, NH3 / 1.) -33 deg C, 0.5 h, 2.) 3 h 2: 99 percent / TsOH / benzene / 10 h / Heating 3: 1.) O3, 2.) NH2OH*HCl / 1.) MeOH, 0 deg C, 2.) 0 deg C, 30 min; reflux 4: 92 percent / H2SO4 / 0.75 h / 125 °C 5: 81 percent / 1,2-dichloro-ethane / 24 h / Ambient temperature View Scheme
参考文献
Russian Journal of Organic Chemistry, , vol. 34, # 2 p. 202 - 204
反应条件
1: 92 percent / H2SO4 / 0.75 h / 125 °C 2: 81 percent / 1,2-dichloro-ethane / 24 h / Ambient temperature View Scheme
参考文献
Russian Journal of Organic Chemistry, , vol. 34, # 2 p. 202 - 204
反应条件
1: 1.) O3, 2.) NH2OH*HCl / 1.) MeOH, 0 deg C, 2.) 0 deg C, 30 min; reflux 2: 92 percent / H2SO4 / 0.75 h / 125 °C 3: 81 percent / 1,2-dichloro-ethane / 24 h / Ambient temperature View Scheme
参考文献
Russian Journal of Organic Chemistry, , vol. 34, # 2 p. 202 - 204
