乙基2-羟基-4-甲基苯甲酸酯合成路线 （共 10 条）
参考文献
Kotschetkow et al.
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1955 , p. 809,813; engl. Ausg. S. 729, 731
Zhurnal Obshchei Khimii, 1959 , vol. 29, p. 650,655; engl. Ausg. S. 643, 646
反应条件
sulfuric acid
16 h; Reflux;
参考文献
ALMIRALL, S.A.; DRACONIS PHARMA, S.L.; LABORATORIOS DEL DR. ESTEVE, S.A.; AGUILAR, Nuria; FERNANDEZ, Joan, Carles; TERRICABRAS, Emma; CARCELLER GONZALEZ, Elena; SALAS SOLANA, Jordi
Patent: WO2013/149997 A1, 2013 ;
Location in patent: Page/Page column 146 ;
反应条件
C10H12INO4 in diethylene glycol dimethyl ether; water
T=40°C; 48 h;
参考文献
Cui, Li-Qian; Dong, Zhi-Lei; Liu, Kai; Zhang, Chi
Organic Letters, 2011 , vol. 13, # 24 p. 6488 - 6491
反应条件
palladium diacetate; 1-fluoro-pyridinium tetrafluoroborate; trifluoroacetic acid; trifluoroacetic anhydride
T=60 - 80°C; 24 h; Sealed tube; regioselective reaction;
参考文献
Rao, Yu
Synlett, 2013 , vol. 24, # 19 p. 2472 - 2476
参考文献
Datta, Apurba; Ila, Hiriyakkanavar; Junjappa, Hiriyakkanavar
Tetrahedron Letters, 1988 , vol. 29, # 4 p. 497 - 500
反应条件
sulfuric acid; sodium hydrogencarbonate; mercury in (2S)-N-methyl-1-phenylpropan-2-amine hydrate; ethanol
参考文献
Chimie, Rhodia
Patent: US6458757 B1, 2002 ;
反应条件
[Ru2(p-PriC6H4Me)2(μ-Cl)Cl]2; 1-(chloromethyl)-4-fluoro-1,4-diazoniabicyclo-[2.2.2]octane bis(tetrafluoroborate); trifluoroacetic acid; trifluoroacetic anhydride
T=80°C; 3 h;
参考文献
Yang, Yiqing; Lin, Yun; Rao, Yu
Organic Letters, 2012 , vol. 14, # 11 p. 2874 - 2877
反应条件
potassium carbonate; toluene
参考文献
Kotschetkow et al.
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1955 , p. 809,813; engl. Ausg. S. 729, 731
Zhurnal Obshchei Khimii, 1959 , vol. 29, p. 650,655; engl. Ausg. S. 643, 646
参考文献
Kotschetkow et al.
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1955 , p. 809,813; engl. Ausg. S. 729, 731
Zhurnal Obshchei Khimii, 1959 , vol. 29, p. 650,655; engl. Ausg. S. 643, 646
反应条件
N-bromosuccinmide; dibenzoyl peroxide in tetrachloromethane
参考文献
Prolinx, Inc.
Patent: US5777148 A1, 1998 ;
