1,3-二甲基-2-碘苯合成路线 （共 73 条）
反应条件
iodine; potassium carbonate in acetonitrile T=80°C; 12 h; Inert atmosphereSchlenk techniqueSealed tube;
参考文献
Niu, Liting; Zhang, Hao; Yang, Haijun; Fu, Hua
Synlett, 2014 , vol. 25, # 7 art. no. 691, p. 995 - 1000
反应条件
Diazotization.Behandlung der Diazoniumsalz-Loesung mit KI;
参考文献
Journal of the American Chemical Society, , vol. 71, p. 1362,1366
Monatshefte fuer Chemie, , vol. 64, p. 361,364, 365
Monatshefte fuer Chemie, , vol. 65, p. 6,14
反应条件
1: in ethylene glycol dimethyl ether 2 h; 2: With iodine in tetrahydrofuran T=20°C; 3 h;
参考文献
Bioorganic and Medicinal Chemistry Letters, , vol. 11, # 3 p. 327 - 329
反应条件
tetrafluoroboric acid; IPy2BF4 in diethyl ether; dichloromethane Ambient temperature; Yield given. Yields of byproduct given;
参考文献
Journal of Organic Chemistry, , vol. 58, # 8 p. 2058 - 2060
反应条件
in tetrahydrofuran 3 h; Heating;
参考文献
Vinod; Hart
Journal of Organic Chemistry, 1990 , vol. 55, # 3 p. 881 - 890
反应条件
1: phenol With sodium hydride in tetrahydrofuran T=20°C; 0.5 h; Inert atmosphere; 2: With copper(l) chloride in tetrahydrofuran T=20°C; 0.5 h; Inert atmosphere; 3: 1,4-diiodo-2,6-dimethylbenzene Further stages;
参考文献
Angewandte Chemie - International Edition, , vol. 49, # 12 p. 2185 - 2189
反应条件
T=25°C; sowie bei 46grad; Equilibrium constant;
参考文献
Journal of the American Chemical Society, , vol. 81, p. 2374,2376
反应条件
2: SOCl2 View Scheme
参考文献
Raaen,V.F.; Eastham,J.F.
Journal of the American Chemical Society, 1960 , vol. 82, p. 1349 - 1352
反应条件
(tBuCN)2CuOTf; silver fluoride in N,N-dimethyl-formamide T=140°C; 22 h; Inert atmosphere;
参考文献
Fier, Patrick S.; Hartwig, John F.
Journal of the American Chemical Society, 2012 , vol. 134, # 26 p. 10795 - 10798
反应条件
1: lithium; diethyl ether / anschliessend Behandeln mit Acetaldehyd 2: activated Al2O3 / 270 - 280 °C / 10 Torr View Scheme
参考文献
Schwartzman; Corson
Journal of the American Chemical Society, 1954 , vol. 76, p. 781,783
