Khan, Khalid Mohammed; Rani, Mubeen; Ambreen, Nida; Ejaz, Asma; Perveen, Shahnaz; Haider, Syed Moazzam; Choudhary, Mohammad Iqbal; Voelter, Wolfgang
Letters in Drug Design and Discovery, 2012 , vol. 9, # 2 p. 135 - 139
3-chloroprop-1-ene; trifluoroacetic acid; cobalt(II) dibromide in acetonitrile Zn dust (1.5 equiv., acid-activated) , CoBr2 (0.1 equiv.), stirred for 5min with allyl chloride (0.3 equiv.), a soln. of aryl halide (1 equiv.) and a soln. 1 equiv. of B compd. added at room temp., stirred for 30 mi n, tranesterificated with pinacol; hydrolized (NH4Cl), extd. (diethyl ether);
参考文献
Claudel, Stephanie; Gosmini, Corinne; Paris, Jean Marc; Perichon, Jacques
Chemical Communications, 2007 , # 35 p. 3667 - 3669
1: copper-powder / 250 - 285 °C / Erwaermen der bei 190-200grad/4 Torr siedenden Anteile des Reaktionsprodukts mit aethanol. Kalilauge
2: quinoline
View Scheme
