2-溴-4-叔丁基-1-甲苯合成路线 （共 13 条）
反应条件
N-bromosuccinmide; dibenzoyl peroxide in tetrachloromethane Heating;
参考文献
Mallory, Frank B; Butler, Kelly E; Berube, Amelie; Luzik Jr., Eddie D; Mallory, Clelia W; Brondyke, Emilie J; Hiremath, Rupa; Ngo, Phung; Carroll, Patrick J
Tetrahedron, 2001 , vol. 57, # 17 p. 3715 - 3724
反应条件
bromine in acetic acid
T=50°C; 120 h;
参考文献
Mallory, Frank B; Butler, Kelly E; Berube, Amelie; Luzik Jr., Eddie D; Mallory, Clelia W; Brondyke, Emilie J; Hiremath, Rupa; Ngo, Phung; Carroll, Patrick J
Tetrahedron, 2001 , vol. 57, # 17 p. 3715 - 3724
反应条件
Sodium bromate; sodium hydrogensulfite in water; acetonitrile
T=20°C; Bromination; 4 h;
参考文献
Kikuchi, Daisuke; Sakaguchi, Satoshi; Ishii, Yasutaka
Journal of Organic Chemistry, 1998 , vol. 63, # 17 p. 6023 - 6026
反应条件
bromine; iodine in water
参考文献
Voskoboynikov, Alexander Z.; Nikulin, Mikhail V.; Tsarev, Aleksey A.; Asachenko, Andrey F.; Babkin, Alexander V.; Giesbrecht, Garth R.; Canich, Jo Ann M.
Patent: US2011/213109 A1, 2011 ;
反应条件
in benzene-d6
byproducts: P(o-tol)3, biaryl, arene; in C6D6 soln. at 70°C; NMR spectroscopy; K(eq) = 2.3(3)E-3;
参考文献
Roy; Hartwig
Journal of the American Chemical Society, 2001 , vol. 123, # 6 p. 1232 - 1233
反应条件
tetrakis(triphenylphosphine) palladium(0); potassium carbonate in 1,4-dioxane; water
Inert atmosphereReflux;
参考文献
Grigg, R. David; Van Hoveln, Ryan; Schomaker, Jennifer M.
Journal of the American Chemical Society, 2012 , vol. 134, # 39 p. 16131 - 16134,4
反应条件
N-bromosuccinmide in water
T=90°C; 0.666667 h; sonication;
参考文献
Heropoulos, Georgios A.; Cravotto, Giancarlo; Screttas, Constantinos G.; Steele, Barry R.
Tetrahedron Letters, 2007 , vol. 48, # 18 p. 3247 - 3250
反应条件
bromine; acetic acid
参考文献
Stock; Brown
Journal of the American Chemical Society, 1959 , vol. 81, p. 5615,5617, 5620
反应条件
N-bromosuccinmide; α,α'-azodiizobutyramidine-dihydrochloride in water
T=80°C; 2 h; Irradiation;
参考文献
Podgorsek, Ajda; Stavber, Stojan; Zupan, Marko; Iskra, Jernej
Tetrahedron, 2009 , vol. 65, # 22 p. 4429 - 4439
参考文献
Stock; Brown
Journal of the American Chemical Society, 1959 , vol. 81, p. 5615,5617, 5620
