2-(1H-吡咯-1-基)苄基乙醇合成路线 (共 7 条)
反应条件
lithium aluminium tetrahydride in diethyl ether 0.25 h;
参考文献
Li, Zhenghua; Kumar, Amit; Vachhani, Dipak D.; Sharma, Sunil K.; Parmar, Virinder S.; Van Der Eycken, Erik V.
European Journal of Organic Chemistry, 2014 , vol. 2014, # 10 p. 2084 - 2091
反应条件
1: With RedAlreg; in toluene T=35 - 45°C; 1 h; 2: With hydrogenchloride in water T=0°C;
参考文献
CEPHALON, INC.; CEPHALON FRANCE
Patent: EP1586559 A1, 2005 ;
Location in patent: Page/Page column 64-65 ;
反应条件
1: K2CO3 / dimethylformamide / Ambient temperature 2: LiAlH4 / tetrahydrofuran View Scheme
参考文献
Journal of Medicinal Chemistry, , vol. 39, # 2 p. 596 - 604
反应条件
1: 80 percent / acetic acid / Heating 2: LAH / diethyl ether / 0 °C View Scheme
参考文献
Chemistry Letters, , # 6 p. 624 - 625
反应条件
manganese(IV) oxide in benzene 16 h; Heating;
参考文献
Garofalo, Antonio; Ragno, Gaetano; Campiani, Giuseppe; Brizzi, Antonella; Nacci, Vito
Tetrahedron, 2000 , vol. 56, # 47 p. 9351 - 9355
反应条件
T=900°C; Cyclization; P=0.01 Torr;
参考文献
Clark, Bernard A. J.; Despinoy, Xavier L. M.; McNab, Hamish; Sommerville, Craig C.; Stevenson, Elizabeth
Journal of the Chemical Society - Perkin Transactions 1, 1999 , # 15 p. 2049 - 2051