反应条件
1: 1.) 95percent tert-butyl hypochlorite, 2.) Et3N / 1.) CH2Cl2, from -70 to -65 deg C, 1 h, 2.) from -65 deg C to RT
2: 3 N aq. HCl / CH2Cl2 / 1 h / Ambient temperature
View Scheme
参考文献
Walsh, David A.; Shamblee, Dwight A.; Welstead, William J.; Sancilio, Lawrence F.
Journal of Medicinal Chemistry, 1982 , vol. 25, # 4 p. 446 - 451
