反应条件
1: sodium hydroxide; thionyl chloride / N,N-dimethyl acetamide; water / 0.42 h / -5 °C / |Inert atmosphere
2: N,N-dimethyl acetamide; water / 1 h / 0 - 20 °C / |Inert atmosphere
View Scheme
参考文献
Shirai, Tomohiko; Ito, Hajime; Yamamoto, Yasunori
Angewandte Chemie - International Edition, 2014 , vol. 53, # 10 p. 2658 - 2661
Angew. Chem., 2014 , vol. 126, # 10 p. 2696 - 2699,4