N,N-二甲基苯甲酰胺合成路线 （共 319 条）
反应条件
bromine in tetrahydrofuran sec-BuONa/complex=5, room temp., then addn. of Br2; not isolated, detd. by gas chromy.;
参考文献
Journal of Organometallic Chemistry, , vol. 361, p. C37 - C40
反应条件
in toluene 3 h; Heating;
参考文献
Russian Chemical Bulletin, , vol. 42, # 11 p. 1848 - 1854
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, , # 11 p. 1932 - 1937
反应条件
potassium permanganate; N-benzyl-N,N,N-trimethyl-ammonium chloride in dichloromethane 3 h; Heating; Yield given. Yields of byproduct given;
参考文献
Synthetic Communications, , vol. 27, # 7 p. 1285 - 1290
反应条件
1: 84 percent / toluene / 24 h / 20 °C 2: 74 percent / MeONa / methanol / 0.25 h / 20 °C 3: 0.067 g / toluene / 3 h / Heating View Scheme
参考文献
Russian Chemical Bulletin, , vol. 42, # 11 p. 1848 - 1854
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, , # 11 p. 1932 - 1937
反应条件
1: 74 percent / MeONa / methanol / 0.25 h / 20 °C 2: 0.067 g / toluene / 3 h / Heating View Scheme
参考文献
Russian Chemical Bulletin, , vol. 42, # 11 p. 1848 - 1854
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, , # 11 p. 1932 - 1937
反应条件
1: 87 percent / diethyl ether / 1 h / Heating 2: 40 percent / benzoylchloride / diethyl ether / 1 h / Heating View Scheme
参考文献
Journal fuer Praktische Chemie (Leipzig), , vol. 328, # 4 p. 567 - 572
反应条件
1: 98 percent / 2-dimethylamino-2,4,6-triphenyl-2H-thiopyrane / diethyl ether / 1 h / Heating 2: 70 percent HClO4 / H2O 3: 87 percent / diethyl ether / 1 h / Heating 4: 40 percent / benzoylchloride / diethyl ether / 1 h / Heating View Scheme
参考文献
Journal fuer Praktische Chemie (Leipzig), , vol. 328, # 4 p. 567 - 572
反应条件
1: 70 percent HClO4 / H2O 2: 87 percent / diethyl ether / 1 h / Heating 3: 40 percent / benzoylchloride / diethyl ether / 1 h / Heating View Scheme
参考文献
Journal fuer Praktische Chemie (Leipzig), , vol. 328, # 4 p. 567 - 572
反应条件
1: 2) Et3N / 1) acetonitrile, 6 h, reflux, 2) C6H6, 1 h 2: benzoyl chloride / CDCl3 / 20 °C View Scheme
参考文献
Chemische Berichte, , vol. 114, # 10 p. 3421 - 3429
反应条件
in tetrahydrofuran LiNMe2/complex=5, CO atm., room temp., 24 h; not isolated, detd. by gas chromy.;
参考文献
Kawasaki, Nobuo; Masuzoe, Kenji; Ozawa, Fumiyuki; Yamamoto, Akio
Journal of Organometallic Chemistry, 1989 , vol. 361, p. C37 - C40
