N,N-二甲基苯甲酰胺合成路线 （共 319 条）
反应条件
thiophosphorylated amine resin in toluene T=90°C; 30 h;
参考文献
Cho, Dongho; Ahn, Jiyoung; De Castro, Kathlia A.; Ahn, Hyunseok; Rhee, Hakjune
Tetrahedron, 2010 , vol. 66, # 30 p. 5583 - 5588
参考文献
Perregaard,J. et al.
Bulletin des Societes Chimiques Belges, 1977 , vol. 86, p. 321 - 328
参考文献
Perregaard,J. et al.
Bulletin des Societes Chimiques Belges, 1977 , vol. 86, p. 321 - 328
参考文献
Kindler
Justus Liebigs Annalen der Chemie, 1923 , vol. 431, p. 213
Chem. Zentralbl., 1923 , vol. 94, # II p. 403
反应条件
1: 1.) samarium(III) trifluoromethanesulfonate, s-butyllithium, hexamethylphosphoric triamide / 1.) THF, cyclohexane, room temperature, 1 h, 2.) THF, cyclohexane, room temperature, 1 h 2: 1.) samarium(III) trifluoromethanesulfonate, s-butyllithium, hexamethylphosphoric triamide / 1.) THF, cyclohexane, room temperature, 1 h, 2.) THF, cyclohexane, room temperature, 1 h View Scheme
参考文献
Fukuzawa, Shin-Ichi; Mutoh, Keisuke; Tsuchimoto, Teruhisa; Hiyama, Tamejiro
Journal of Organic Chemistry, 1996 , vol. 61, # 16 p. 5400 - 5405
反应条件
n-butyllithium; 2-(dimethylamino)-ethanol 1.) hexane, -78 deg C, 1 h, 2.) THF, -78 deg C, 1 h;
参考文献
Gros, Philippe; Fort, Yves; Caubere, Paul
Journal of the Chemical Society - Perkin Transactions 1, 1997 , # 24 p. 3597 - 3600
反应条件
in tetrahydrofuran 1 h; Inert atmosphere;
参考文献
Rao, G. Venkateswara; Swamy, B. Narayana; Kumar, P. Hareesh; Reddy, G. Chandrasekara
Synthetic Communications, 2009 , vol. 39, # 10 p. 1835 - 1846
反应条件
[RuIII(2,4-pentanedionato)3]; methanesulfonic acid; hydrogen; 1,1,1-tris (diphenylphosphinomethyl)ethane in tetrahydrofuran T=220°C; P=7500.75 Torr; 16 h; AutoclaveInert atmosphere;
参考文献
Coetzee, Jacorien; Dodds, Deborah L.; Klankermayer, Juergen; Brosinski, Sandra; Leitner, Walter; Slawin, Alexandra M. Z.; Cole-Hamilton, David J.
Chemistry - A European Journal, 2013 , vol. 19, # 33 p. 11039 - 11050
反应条件
cis-[Ru(CH3CN)2(η3-C3H5)(cod)]BF4; hydrogen; potassium hexamethylsilazane; 2-(diphenylphosphino)ethylamine in tetrahydrofuran T=100°C; P=38002.6 Torr; 24 h; Autoclave;
参考文献
John, Jeremy M.; Bergens, Steven H.
Angewandte Chemie - International Edition, 2011 , vol. 50, # 44 p. 10377 - 10380
反应条件
tri-ruthenium(0)dodecacarbonyl; hydrogen; molybdenum hexacarbonate in ethylene glycol dimethyl ether T=160°C; P=75007.5 Torr; 16 h; Inert atmosphere;
参考文献
Advanced Synthesis and Catalysis, , vol. 352, # 5 p. 869 - 883
