N,N-二甲基苯甲酰胺合成路线 （共 319 条）
反应条件
bis(1,5-cyclooctanediylboryl)monoselenide in dichloromethane; benzene 18 h; Heatingother solvent, temperature, reaction time; Product distribution;
参考文献
Bulletin of the Chemical Society of Japan, , vol. 70, # 1 p. 197 - 206
反应条件
trichlorophosphate CH3CN, 30 min, reflux; Yield given. Multistep reaction;
参考文献
Harris, Roger L.N.
Synthesis, 1980 , # 10 p. 841 - 842
反应条件
lithium; p-benozquinone 1) THF, 0 deg C, 2) CH2Cl2, 0 deg C, 3 h; Yield given. Multistep reaction;
参考文献
Barrett, Anthony G. M.; Dauzonne, Daniel; O'Neil, Ian A.; Renaud, Alain
Journal of Organic Chemistry, 1984 , vol. 49, # 23 p. 4409 - 4415
反应条件
[Re2(CO)10] in toluene T=180°C; 24 h;
参考文献
Angewandte Chemie - International Edition, , vol. 52, # 45 p. 11879 - 11883
Angew. Chem., , p. 12095 - 12099
反应条件
trichlorophosphate in dichloromethane T=25°C; 18 h;
参考文献
Harris, Roger L. N.
Synthesis, 1981 , # 11 p. 907 - 908
反应条件
hydrogenchloride 1.) THF, 4 h, reflux; Yield given. Multistep reaction;
参考文献
Synthesis, , # 3 p. 228 - 230
反应条件
[RuIII(2,4-pentanedionato)3]; methanesulfonic acid; hydrogen; 1,1,1-tris (diphenylphosphinomethyl)ethane in tetrahydrofuran T=220°C; P=7500.75 Torr; 16 h; AutoclaveInert atmosphere;
参考文献
Coetzee, Jacorien; Dodds, Deborah L.; Klankermayer, Juergen; Brosinski, Sandra; Leitner, Walter; Slawin, Alexandra M. Z.; Cole-Hamilton, David J.
Chemistry - A European Journal, 2013 , vol. 19, # 33 p. 11039 - 11050
反应条件
1: 2-bromo-1-[2-(trimethylsilyl)ethynyl]benzene With tert.-butyl lithium in tetrahydrofuran T=-78°C; 0.5 h; Inert atmosphere; 2: N,N-dimethyl benzamide in tetrahydrofuran T=-78 - 20°C; Inert atmosphere; 3: With hydrogenchloride; water in acetone T=20°C; 1 h; Inert atmosphere;
参考文献
Katsumoto, Kenta; Kitamura, Chitoshi; Kawase, Takeshi
European Journal of Organic Chemistry, 2011 , # 25 p. 4885 - 4891
反应条件
[bis(acetoxy)iodo]benzene; [Ru(p-cymene)(MesCO2)2]; trifluoroacetic acid; trifluoroacetic anhydride T=120°C; 30 h;
参考文献
Thirunavukkarasu, Vedhagiri S.; Hubrich, Jonathan; Ackermann, Lutz
Organic Letters, 2012 , vol. 14, # 16 p. 4210 - 4213
反应条件
1: methylene cyclopropane With n-butyllithium in tetrahydrofuran T=-10 - 10°C; 2 h; 2: N,N-dimethyl benzamide in tetrahydrofuran T=-78°C; 2 h;
参考文献
Ma, Shengming; Lu, Lianghua; Zhang, Junliang
Journal of the American Chemical Society, 2004 , vol. 126, # 31 p. 9645 - 9660
