N,N-二甲基苯甲酰胺合成路线 （共 319 条）
反应条件
1: CH2Cl2 / 0.5 h / 0 °C
2: 2,6-di-tert-butylpyridine / 0.5 h / Ambient temperature
3: aq. NaHCO3 / 0.25 h
View Scheme
参考文献
Sforza, Stefano; Dossena, Arnaldo; Corradini, Roberto; Virgili, Eliana; Marchelli, Rosangela
Tetrahedron Letters, 1998 , vol. 39, # 7 p. 711 - 714
反应条件
silver hexafluoroantimonate; [{(η5-C5Me5)RhCl}2(μ-Cl)2]; silver carbonate in tetrahydrofuran
T=110°C; 20 h; Inert atmosphere; regioselective reaction;
参考文献
Park, Jihye; Park, Eonjeong; Kim, Aejin; Lee, Youngil; Chi, Ki-Whan; Kwak, Jong Hwan; Jung, Young Hoon; Kim, In Su
Organic Letters, 2011 , vol. 13, # 16 p. 4390 - 4393
反应条件
1: N-methyl-2-phenylaziridine With sec.-butyllithium in tetrahydrofuran; cyclohexane
T=-78°C; 2 h;
2: N,N-dimethyl benzamide in tetrahydrofuran; cyclohexane
T=-78 - 20°C;
参考文献
Capriati, Vito; Florio, Saverio; Luisi, Renzo; Musio, Biagia
Organic Letters, 2005 , vol. 7, # 17 p. 3749 - 3752
反应条件
N,N,N',N,-tetramethylethylenediamine in tetrahydrofuran
T=-78°C; 1 h;
参考文献
Beak, Peter; Brown, Roger A.
Journal of Organic Chemistry, 1982 , vol. 47, # 1 p. 34 - 46
反应条件
[RuIII(2,4-pentanedionato)3]; methanesulfonic acid; hydrogen; 1,1,1-tris (diphenylphosphinomethyl)ethane in tetrahydrofuran
T=220°C; P=7500.75 Torr; 16 h; AutoclaveInert atmosphere;
参考文献
Coetzee, Jacorien; Dodds, Deborah L.; Klankermayer, Juergen; Brosinski, Sandra; Leitner, Walter; Slawin, Alexandra M. Z.; Cole-Hamilton, David J.
Chemistry - A European Journal, 2013 , vol. 19, # 33 p. 11039 - 11050
反应条件
PPA; sodium acetate; trichlorophosphate
Yield given. Multistep reaction;
参考文献
Carson, John R.; Davis, Nancy M.
Journal of Organic Chemistry, 1981 , vol. 46, # 5 p. 839 - 843
反应条件
sodium acetate; trichlorophosphate
Yield given. Multistep reaction. Title compound not separated from byproducts;
参考文献
Carson, John R.; Davis, Nancy M.
Journal of Organic Chemistry, 1981 , vol. 46, # 5 p. 839 - 843
反应条件
1: 1.) tert-BuLi, TMEDA / 1.) -70 deg C
2: 91 percent / acetic acid / 3 h / Heating
View Scheme
参考文献
Ohta; Kamata; Inagaki; Masuda; Yamamoto; Yamashita; Kawasaki
Chemical and Pharmaceutical Bulletin, 1993 , vol. 41, # 6 p. 1188 - 1190
反应条件
1: N,N-dimethyl benzamide With PhMe2SiLi in tetrahydrofuran
T=-20°C; 1 h;
2: chloroformic acid ethyl ester in tetrahydrofuran
T=-20 - 20°C;
参考文献
Fleming, Ian; Russell, Matthew G.
Chemical Communications, 2003 , # 2 p. 198 - 199
反应条件
1: phosphorus oxychloride / 0.03 h / 100 °C
2: CHCl3 / 48 h / Ambient temperature
View Scheme
参考文献
Harris, Roger L. N.
Australian Journal of Chemistry, 1981 , vol. 34, # 3 p. 623 - 634
