N,N-二甲基苯甲酰胺合成路线 （共 319 条）
反应条件
bis(1,5-cyclooctanediylboryl)monoselenide in dichloromethane; benzene
18 h; Heatingother solvent, temperature, reaction time; Product distribution;
参考文献
Shimada, Kazuaki; Jin, Norikazu; Kawaguchi, Michiko; Dobashi, Kumiko; Nagano, Yumi; Fujimura, Manabu; Kudoh, Eiichi; Kai, Tomonari; Saito, Noboru; Masuda, Jun-Ichi; Iwaya, Masaki; Fujisawa, Hiroyuki; Aoyagi, Shigenobu; Takikawa, Yuji
Bulletin of the Chemical Society of Japan, 1997 , vol. 70, # 1 p. 197 - 206
反应条件
1.1: BuLi / tetrahydrofuran; hexane / 0.17 h / -78 °C
1.2: 81 percent / tetrahydrofuran; hexane / 0.08 h / -78 °C
2.1: anisole; TFA / CH2Cl2 / 0.75 h
View Scheme
参考文献
Fraser, David S.; Park, Sheldon B.; Chong, J. Michael
Canadian Journal of Chemistry, 2004 , vol. 82, # 2 p. 87 - 101
参考文献
Taverne
Recueil des Travaux Chimiques des Pays-Bas, 1898 , vol. 17, p. 193
反应条件
n-butyllithium; borane-THF; diisopropylamine
T=25°C;
参考文献
Fisher, Gary B.; Fuller, Joseph C.; Harrison, John; Goralski, Christian T.; Singaram, Bakthan
Tetrahedron Letters, 1993 , vol. 34, # 7 p. 1091 - 1094
反应条件
sodium diethylpiperidinohydroaluminate in tetrahydrofuran
T=0°C; 24 h;
参考文献
Yoon, Nung Min; Ahn, Jin Hee; An, Duk Keun; Shon, Young Seok
Journal of Organic Chemistry, 1993 , vol. 58, # 7 p. 1941 - 1944
反应条件
1: With lithium aluminium tetrahydride in tetrahydrofuran
T=0°C; 1.5 h;
2: With ammonia; iodine in tetrahydrofuran; water
T=0 - 20°C; 2 h;
参考文献
Suzuki, Yusuke; Yoshino, Takumi; Moriyama, Katsuhiko; Togo, Hideo
Tetrahedron, 2011 , vol. 67, # 21 p. 3809 - 3814
反应条件
cis-[Ru(CH3CN)2(η3-C3H5)(cod)]BF4; hydrogen; potassium hexamethylsilazane; 2-(diphenylphosphino)ethylamine in tetrahydrofuran
T=100°C; P=38002.6 Torr; 24 h; Autoclave;
参考文献
John, Jeremy M.; Bergens, Steven H.
Angewandte Chemie - International Edition, 2011 , vol. 50, # 44 p. 10377 - 10380
参考文献
Taverne
Recueil des Travaux Chimiques des Pays-Bas, 1898 , vol. 17, p. 193
反应条件
water; trifluoroacetic acid
T=99°C; determined by 1H NMR; Rate constant;
参考文献
Wagenaar, Anno; Kirby, Anthony J.; Engberts, Jan B. F. N.
Recueil des Travaux Chimiques des Pays-Bas, 1985 , vol. 104, # 7-8 p. 203 - 205
