(6-甲氧基-1-萘基)甲醇合成路线 （共 12 条）
反应条件
lithium aluminium tetrahydride in tetrahydrofuran
4 h; Heating;
参考文献
Gaur, S. P.; Jain, Padam C.; Anand, Nitya
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1982 , vol. 21, # 1 p. 46 - 51
反应条件
1: 19 g / AlCl3
2: 20.4 g / LAH / tetrahydrofuran / 4h, r.t.
View Scheme
参考文献
Dutt, Sachchidananda; Banerjee, Amalendu; Karmarkar, Tapan K.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1982 , vol. 21, # 3 p. 192 - 196
反应条件
1: 19 g / AlCl3
2: 20.4 g / LAH / tetrahydrofuran / 4h, r.t.
View Scheme
参考文献
Dutt, Sachchidananda; Banerjee, Amalendu; Karmarkar, Tapan K.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1982 , vol. 21, # 3 p. 192 - 196
反应条件
lithium aluminium tetrahydride in tetrahydrofuran
4h, r.t.;
参考文献
Dutt, Sachchidananda; Banerjee, Amalendu; Karmarkar, Tapan K.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1982 , vol. 21, # 3 p. 192 - 196
反应条件
diisobutylaluminium hydride in toluene; benzene
参考文献
Neef; Eder; Haffer; et al.
Chemische Berichte, 1976 , vol. 109, # 9 p. 3025 - 3033
参考文献
Schreiber,K.C.; Byers,R.G.
Journal of the American Chemical Society, 1962 , vol. 84, p. 859 - 862
反应条件
diethyl ether; magnesium; benzene
weiteres Reagens: Aethylbromid; Einleiten von Formaldehyd in die gekuehlte Reaktionsloesung;
参考文献
Billeter; Miescher
Helvetica Chimica Acta, 1946 , vol. 29, p. 859,865
反应条件
1: 85.1 percent / MnO2 / benzene / 6 h / Heating
2: 88.6 percent / piperidine acetate / toluene / Heating
3: 90 percent / LiAlH4 / tetrahydrofuran / Heating
4: 50percent aq. sulphuric acid / a. water removed, b. 130-140 deg C (15mm), 2h
5: 10percent aq. NaOH / Heating
6: 82.3 percent / Heating
7: POCl3 / toluene / 95 °C
8: NaBH4 / methanol / Ambient temperature
View Scheme
参考文献
Gaur, S. P.; Jain, Padam C.; Anand, Nitya
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1982 , vol. 21, # 1 p. 46 - 51
反应条件
1: 85.1 percent / MnO2 / benzene / 6 h / Heating
2: 88.6 percent / piperidine acetate / toluene / Heating
View Scheme
参考文献
Gaur, S. P.; Jain, Padam C.; Anand, Nitya
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1982 , vol. 21, # 1 p. 46 - 51
反应条件
phosphorus tribromide in benzene
12 h; Ambient temperature;
参考文献
Mukerjee, Y. N.; Gaur, S. P.; Jain, P. C.; Anand, Nitya
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1985 , vol. 24, p. 985 - 987
