顺式-1,2-二羟甲基乙烯合成路线 （共 151 条）
反应条件
4-(N,N-dimethlyamino)pyridine; triethylamine in dichloromethane
T=20°C; 24 h;
参考文献
Hernandez, Ana-Isabel; Familiar, Olga; Negri, Ana; Rodriguez-Barrios, Fatima; Gago, Federico; Karlsson, Anna; Camarasa, Maria-Jose; Balzarini, Jan; Perez-Perez, Maria-Jesus
Journal of Medicinal Chemistry, 2006 , vol. 49, # 26 p. 7766 - 7773
反应条件
n-butyllithium in tetrahydrofuran; hexane
T=-78 - 20°C; 2 h; Yields of byproduct given;
参考文献
Roush, William R.; Reilly, Melissa L.; Koyama, Kazuo; Brown, Bradley B.
Journal of Organic Chemistry, 1997 , vol. 62, # 25 p. 8708 - 8721
反应条件
3-chloro-benzenecarboperoxoic acid
Epoxidation;
参考文献
Wu, Michael H.; Hansen, Karl B.; Jacobsen, Eric N.
Angewandte Chemie - International Edition, 1999 , vol. 38, # 13-14 p. 2012 - 2014
反应条件
toluene-4-sulfonic acid in benzene
Heating;
参考文献
Abuzov, B. A.; Klimovitskii, E. N.; Remizov, A. B.; Timirbaev, M. B.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1981 , vol. 30, # 5 p. 794 - 799
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1981 , # 5 p. 1030 - 1036
反应条件
C55H58ClN3ORu; phenyl-trichloro-silane in toluene
T=50°C; 5 h;
参考文献
Behr, Arno; Gomes, Jessica Perez
Beilstein Journal of Organic Chemistry, 2011 , vol. 7, p. 1 - 8
反应条件
[Rh(OH)(cycloocta-1,5-diene)]2 in 1,4-dioxane
T=20°C; 12 h;
参考文献
Miura, Tomoya; Takahashi, Yusuke; Murakami, Masahiro
Chemical Communications, 2007 , # 6 p. 595 - 597
反应条件
pyridine; diphosphinidenecyclobutene-coordinated palladium in toluene
T=100°C; 2.5 h;
参考文献
Murakami, Hiromi; Matsui, Yukio; Ozawa, Fumiyuki; Yoshifuji, Masaaki
Journal of Organometallic Chemistry, 2006 , vol. 691, # 14 p. 3151 - 3156
反应条件
toluene-4-sulfonic acid
参考文献
Pattison
Journal of Organic Chemistry, 1957 , vol. 22, p. 662
反应条件
1,2,3-Benzotriazole; thionyl chloride in dichloromethane
T=20°C; Cyclization;
参考文献
Chaudhari, Sachin S.; Akamanchi, Krishnacharya G.
Synlett, 1999 , # 11 p. 1763 - 1765
反应条件
4,4'-diaminostilbene-2,2'-disulfonic acid in dichloromethane
0.5 h; Further byproducts given. Yields of byproduct given;
参考文献
Shellhamer, Dale F.; Anstine, D. Timothy; Gallego, Kelly M.; Ganesh, Brian R.; Hanson, Aaron A.; et al.
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1995 , # 4 p. 861 - 866
