1: methyl iodide With Sn[N(SiMe3)2]2 in tetrahydrofuran T=20°C; 0.0833333 h; 2: With tetrabutyl ammonium fluoride in tetrahydrofuran T=20°C; 3: 2-bromo-naphthalene With triphenylphosphine; tris-(dibenzylideneacetone)dipalladium(0) in 1,4-dioxane 4 h; Heating; Further stages.;
1: With gallium(III) chloride T=70°C; 40 h; 2: With 1-methyl-naphthalene; palladium on activated charcoal 2 h; Heating; 3: With 2,3-dicyano-5,6-dichloro-p-benzoquinone in toluene 3 h; Heating;
参考文献
Journal of Organic Chemistry, , vol. 68, # 17 p. 6752 - 6759