1-环己基-4-甲氧基苯合成路线 （共 57 条）
反应条件
digallium tetrachloride in carbon disulfide
24 h; Heating; Yield given. Yields of byproduct given;
参考文献
Hashimoto, Yukihiko; Hirata, Kazujuki; Kagoshima, Hirotaka; Kihara, Nobuhiro; Hasegawa, Masaki; Saigo, Kazuhiko
Tetrahedron, 1993 , vol. 49, # 27 p. 5969 - 5978
反应条件
in 2,2,2-trifluoroethanol
26 h; Irradiation;
参考文献
Protti, Stefano; Fagnoni, Maurizio; Mella, Mariella; Albini, Angelo
Journal of Organic Chemistry, 2004 , vol. 69, # 10 p. 3465 - 3473
反应条件
C64H60Cl2N12Pd2(2+)*2F6P(1+) in tetrahydrofuran
T=20°C; Kumada-Corriu coupling; 7 h; Inert atmosphere;
参考文献
Chang, Yung-Hung; Liu, Zu-Yin; Liu, Yi-Hung; Peng, Shei-Ming; Chen, Jwu-Ting; Liu, Shiuh-Tzung
Dalton Transactions, 2011 , vol. 40, # 2 p. 489 - 494
反应条件
C64H60Cl2N12Pd2(2+)*2F6P(1+) in tetrahydrofuran
T=20°C; Kumada-Corriu coupling; 5 h; Inert atmosphere;
参考文献
Chang, Yung-Hung; Liu, Zu-Yin; Liu, Yi-Hung; Peng, Shei-Ming; Chen, Jwu-Ting; Liu, Shiuh-Tzung
Dalton Transactions, 2011 , vol. 40, # 2 p. 489 - 494
参考文献
Dodds et al.
Proceedings of the Royal Society of London, Series B: Biological Sciences, 1953 , vol. 140, p. 470,478
反应条件
digallium tetrachloride in carbon disulfide
48 h; Ambient temperature; Yield given. Yields of byproduct given;
参考文献
Hashimoto, Yukihiko; Hirata, Kazujuki; Kagoshima, Hirotaka; Kihara, Nobuhiro; Hasegawa, Masaki; Saigo, Kazuhiko
Tetrahedron, 1993 , vol. 49, # 27 p. 5969 - 5978
反应条件
1: concentrated hydrochloric acid
2: bei der Destillation unter gewoehnlichem Druck oder bei langsamer Destillation unter 250 mm Druck
3: concentrated hydrochloric acid
4: alkali
View Scheme
参考文献
v.Braun
Justus Liebigs Annalen der Chemie, 1929 , vol. 472, p. 34
反应条件
scandium tris(trifluoromethanesulfonate) in tetrachloromethane
T=80°C; 1 h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Kotsuki, Hiyoshizo; Oshisi, Takeshi; Inoue, Motoshi
Synlett, 1998 , # 3 p. 255 - 256
参考文献
Meyer,H.; Bernhauer
Monatshefte fuer Chemie, 1929 , vol. 53/54, p. 728
Full Text Show Details
Bodroux
Annales de Chimie (Cachan, France), 1929 , vol. <10> 11, p. 519,525
Comptes Rendus Hebdomadaires des Seances de l'Academie des Sciences, 1928 , vol. 186, p. 1005
Full Text Show Details
v.Braun
Justus Liebigs Annalen der Chemie, 1929 , vol. 472, p. 34
反应条件
T=150°C; P=73550.8 - 147102 Torr; Hydrogenation;
参考文献
Musser; Adkins
Journal of the American Chemical Society, 1938 , vol. 60, p. 664,666
