戊烷-2,3,4-三酮 3-苯基腙合成路线 （共 21 条）
参考文献
Beyer; Claisen
Chemische Berichte, 1888 , vol. 21, p. 1702
参考文献
Benary; Reiter; Soenderop
Chemische Berichte, 1917 , vol. 50, p. 88
反应条件
hydrazine hydrate; acetic acid
Heating;
参考文献
Kaymakcioglu, Bedia Kocyigit; Rollas, Sevim; Koercegez, Eylem; Aricioglu, Feyza
European Journal of Pharmaceutical Sciences, 2005 , vol. 26, # 1 p. 97 - 103
反应条件
in N,N-dimethyl-formamide
0.1 h; microwave irradiation;
参考文献
Mohamed, Nadia Ragab; El-Saidi, Manal Mohamed Talaat; Ali, Yasser Mahmoud; Elnagdi, Mohamed Hilmy
Journal of Heterocyclic Chemistry, 2007 , vol. 44, # 6 p. 1333 - 1337
反应条件
in benzene
3 h; Heating;
参考文献
Bestmann, Hans Juergen; Schmid, Guenter; Sandmeier, Dieter
Tetrahedron Letters, 1980 , vol. 21, p. 2939 - 2942
反应条件
in toluene
10 h; Heating;
参考文献
Nada, Afaf Aly; Erian, Ayman Wahba; Mohamed, Nadia Ragab; Mahran, Asma Mohamed
Journal of Chemical Research, Miniprint, 1997 , # 7 p. 1576 - 1594
反应条件
sodium hydride
1.) THF, 25 deg C, 2 h, 2.) THF, a.) 25 deg C, 1.5 h, b.) 65 deg C, 8 h; Yield given. Multistep reaction;
参考文献
Patel; Vyas; Pandey; Tavares; Fernandes
Synthetic Communications, 1991 , vol. 21, # 8-9 p. 1021 - 1026
反应条件
LiN(Cy)2
1.) THF, -78 deg C, 15 min, 2.) THF, from -78 deg C to 25 deg C, 4.5 h; Yield given. Multistep reaction;
参考文献
Patel; Vyas; Pandey; Tavares; Fernandes
Synthetic Communications, 1991 , vol. 21, # 18-19 p. 1935 - 1940
反应条件
T=370.2°C; var. temp., further with cyclohexene, Ea; Rate constantThermodynamic dataProduct distribution;
参考文献
Al-Awadi, Nouria A.; El-Nagdi, Mohamed H.; Mathew, Tommy
International Journal of Chemical Kinetics, 1995 , vol. 27, # 5 p. 517 - 524
参考文献
Russell
Journal of the American Chemical Society, 1953 , vol. 75, p. 5315,5319
