2,2-二氯乙酰乙酸乙酯合成路线 (共 16 条)
参考文献
Conrad
Justus Liebigs Annalen der Chemie, 1877 , vol. 186, p. 241
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v. Mayer; Janny
Chemische Berichte, 1882 , vol. 15, p. 1165
参考文献
James
Justus Liebigs Annalen der Chemie, 1887 , vol. 240, p. 64
参考文献
Justus Liebigs Annalen der Chemie, , vol. 186, p. 241
Chemische Berichte, , vol. 20, p. 3057
参考文献
James
Justus Liebigs Annalen der Chemie, 1887 , vol. 240, p. 64
反应条件
ethanol; sodium in diethyl ether 0 deg C, 30 min, reflux, 4 h;
参考文献
Bulletin of the Chemical Society of Japan, , vol. 60, # 7 p. 2475 - 2479
反应条件
ethanol; sodium in diethyl ether 0 deg C, 30 min, reflux, 4 h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Bulletin of the Chemical Society of Japan, , vol. 60, # 7 p. 2475 - 2479
反应条件
trichloroisocyanuric acid in water; acetone
T=20°C; 15 h;
参考文献
Mendonca, Gabriela F.; Sindra, Haryadylla C.; de Almeida, Leonardo S.; Esteves, Pierre M.; de Mattos, Marcio C.S.
Tetrahedron Letters, 2009 , vol. 50, # 4 p. 473 - 475
反应条件
1,5-diazabicyclo[5.4.0]undeca-5-ene in dichloromethane
1:1 molar mixture of educts per acidic hydrogen, 20-25°C, 1 h;
参考文献
Gmelin Handbook: F: PerFHalOrg.SVol.3, 6.2.3.4, page 152 - 186
反应条件
in dichloromethane
1:1 molar mixture of educts per acidic hydrogen, 20-25°C, 1 h;
参考文献
Gmelin Handbook: F: PerFHalOrg.SVol.3, 6.2.3.4, page 152 - 186
反应条件
potassium peroxymonosulfate; ammonium chloride in methanol
T=20°C; 6 h;
参考文献
Swamy, Peraka; Kumar, MacHarla Arun; Reddy, Marri Mahender; Narender, Nama
Chemistry Letters, 2012 , vol. 41, # 4 p. 432 - 434