1: K2CO3 / acetone / 16 h / Heating
2: LiAlH4 / tetrahydrofuran / 30 °C
3: 90 percent / pyridinium chlorochromate / CH2Cl2 / 1 h
View Scheme
参考文献
Zhuravel, Michael A.; Davis, Nicolynn E.; Nguyen, SonBinh T.; Koltover, Ilya
Journal of the American Chemical Society, 2004 , vol. 126, # 32 p. 9882 - 9883
1: LiAlH4 / tetrahydrofuran / 30 °C
2: 90 percent / pyridinium chlorochromate / CH2Cl2 / 1 h
View Scheme
参考文献
Zhuravel, Michael A.; Davis, Nicolynn E.; Nguyen, SonBinh T.; Koltover, Ilya
Journal of the American Chemical Society, 2004 , vol. 126, # 32 p. 9882 - 9883
1: 99 percent / K2CO3 / dimethylformamide / 5 h / 75 °C
2: 95 percent / LiAlH4 / tetrahydrofuran / 0 - 20 °C
3: pyridinium chlorochromate / CH2Cl2 / 20 °C
View Scheme
参考文献
Percec, Virgil; Peterca, Mihai; Sienkowska, Monika J.; Ilies, Marc A.; Aqad, Emad; Smidrkal, Jan; Heiney, Paul A.
Journal of the American Chemical Society, 2006 , vol. 128, # 10 p. 3324 - 3334
1: 99 percent / K2CO3 / dimethylformamide / 5 h / 75 °C
2: 95 percent / LiAlH4 / tetrahydrofuran / 0 - 20 °C
3: pyridinium chlorochromate / CH2Cl2 / 20 °C
View Scheme
参考文献
Percec, Virgil; Peterca, Mihai; Sienkowska, Monika J.; Ilies, Marc A.; Aqad, Emad; Smidrkal, Jan; Heiney, Paul A.
Journal of the American Chemical Society, 2006 , vol. 128, # 10 p. 3324 - 3334
1: K2CO3 / acetone / 16 h / Heating
2: LiAlH4 / tetrahydrofuran / 30 °C
3: 90 percent / pyridinium chlorochromate / CH2Cl2 / 1 h
View Scheme
参考文献
Zhuravel, Michael A.; Davis, Nicolynn E.; Nguyen, SonBinh T.; Koltover, Ilya
Journal of the American Chemical Society, 2004 , vol. 126, # 32 p. 9882 - 9883