反应条件
in methanol; dichloromethane soln. of Co(CH3COO)2*4H2O in MeOH was added to soln. of ligand in CH2Cl2under N2, rinsed with MeOH, stirred for 15 min at room temp., for 30 mi n at 0°C; filtered, rinsed with cold MeOH, collected, dried in vacuo;
参考文献
Schaus, Scott E.; Brandes, Bridget D.; Larrow, Jay F.; Tokunaga, Makoto; Hansen, Karl B.; Gould, Alexandra E.; Furrow, Michael E.; Jacobsen, Eric N.
Journal of the American Chemical Society, 2002 , vol. 124, # 7 p. 1307 - 1315
