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乙二醇
甲醛
63148-62-9
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二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
2-碘代甲苯
合成路线
（共 446 条）
615-37-2
2-碘代甲苯
+
75-20-7
电石
→
反应条件
5294-03-1
反应条件
copper(l) iodide; palladium diacetate; triethylamine; triphenylphosphine in acetonitrile T=20°C; Sonogashira coupling; Inert atmosphere;
参考文献
Chuentragool, Padon; Vongnam, Kunnigar; Rashatasakhon, Paitoon; Sukwattanasinitt, Mongkol; Wacharasindhu, Sumrit
Tetrahedron, 2011 , vol. 67, # 42 p. 8177 - 8182
615-37-2
2-碘代甲苯
+
766-47-2
→
反应条件
5294-03-1
反应条件
bis-(pyridin-2-yl)amine; Pd(NH3)2Cl2; triethylamine in water T=25°C; Sonogashira Cross-Coupling; 6 h; Inert atmosphere;
参考文献
Zhong, Hong; Wang, Jinyun; Li, Liuyi; Wang, Ruihu
Dalton Transactions, 2014 , vol. 43, # 5 p. 2098 - 2103
615-37-2
2-碘代甲苯
+
471-25-0
→
反应条件
136053-56-0
+
5294-03-1
反应条件
bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; potassium carbonate; 1,8-diazabicyclo[5.4.0]undec-7-ene; 1,4-di(diphenylphosphino)-butane in dimethyl sulfoxide T=30 - 80°C; 9 h; DarknessAerobic condition;
参考文献
Kim, Yong; Park, Ahbyeol; Park, Kyungho; Lee, Sunwoo
Tetrahedron Letters, 2011 , vol. 52, # 15 p. 1766 - 1769
615-37-2
2-碘代甲苯
+
74-86-2
→
反应条件
5294-03-1
反应条件
piperidine; copper(l) iodide; tetrakis(triphenylphosphine) palladium(0) T=80°C; Addition; 0.25 h;
参考文献
Stara, Irena G.; Stary, Ivo; Kollarovic, Adrian; Teply, Filip; Saman, David; Fiedler, Pavel
Collection of Czechoslovak Chemical Communications, 1999 , vol. 64, # 4 p. 649 - 672
615-37-2
2-碘代甲苯
+
471-25-0
→
反应条件
5294-03-1
反应条件
bis-triphenylphosphine-palladium(II) chloride; 1,8-diazabicyclo[5.4.0]undec-7-ene; 1,4-di(diphenylphosphino)-butane in dimethyl sulfoxide T=80°C; 3 h;
参考文献
Park, Kyungho; Bae, Goun; Moon, Jeongju; Choe, Jaehoon; Song, Kwang Ho; Lee, Sunwoo
Journal of Organic Chemistry, 2010 , vol. 75, # 18 p. 6244 - 6251
615-37-2
2-碘代甲苯
+
142-45-0
→
反应条件
5294-03-1
反应条件
bis-triphenylphosphine-palladium(II) chloride; 1,8-diazabicyclo[5.4.0]undec-7-ene; 1,4-di(diphenylphosphino)-butane in dimethyl sulfoxide T=110°C; 3 h;
参考文献
Park, Kyungho; Bae, Goun; Moon, Jeongju; Choe, Jaehoon; Song, Kwang Ho; Lee, Sunwoo
Journal of Organic Chemistry, 2010 , vol. 75, # 18 p. 6244 - 6251
615-37-2
2-碘代甲苯
+
1066-54-2
→
反应条件
5294-03-1
+
3989-15-9
反应条件
sodium hydroxide; copper(l) iodide; tetrakis(triphenylphosphine) palladium(0); N-benzyl-N,N,N-triethylammonium chloride in benzene T=40°C; 48 h;
参考文献
D'Auria
Synthetic Communications, 1992 , vol. 22, # 16 p. 2393 - 2399
626-55-1
+
615-37-2
2-碘代甲苯
+
471-25-0
→
反应条件
5294-03-1
反应条件
bis-triphenylphosphine-palladium(II) chloride; 1,8-diazabicyclo[5.4.0]undec-7-ene; 1,4-di(diphenylphosphino)-butane in dimethyl sulfoxide T=50 - 80°C;
参考文献
Park, Kyungho; Bae, Goun; Moon, Jeongju; Choe, Jaehoon; Song, Kwang Ho; Lee, Sunwoo
Journal of Organic Chemistry, 2010 , vol. 75, # 18 p. 6244 - 6251
615-37-2
2-碘代甲苯
+
536-74-3
→
反应条件
5294-03-1
反应条件
potassium acetate in dimethyl sulfoxide T=110°C; Sonogashira coupling; 4 h;
参考文献
Shao, Linjun; Ji, Weixin; Dong, Pengdu; Zeng, Minfeng; Qi, Chenze; Zhang, Xian-Man
Applied Catalysis A: General, 2012 , vol. 413-414, p. 267 - 272
615-37-2
2-碘代甲苯
→
反应条件
5294-03-1
反应条件
1: copper(l) iodide; bis-triphenylphosphine-palladium(II) chloride; triethylamine / 120 h / Inert atmosphere 2: tetrabutyl ammonium fluoride / tetrahydrofuran / -78 - 20 °C / Inert atmosphere 3: copper(l) iodide; bis-triphenylphosphine-palladium(II) chloride; triethylamine / 120 h / Inert atmosphere View Scheme
参考文献
Weisheit, Thomas; Escudero, Danie; Petzold, Holm; Goerls, Helmar; Gonzalez, Leticia; Weigand, Wolfgang
Dalton Transactions, 2010 , vol. 39, # 40 p. 9493 - 9504
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