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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
2-碘苯胺
合成路线
（共 712 条）
615-43-0
2-碘苯胺
+
93-91-4
1-苯基-1,3-丁二酮
→
反应条件
26211-73-4
(2-甲基-1H-吲哚-3-基)(苯基)甲酮
反应条件
copper(l) iodide; caesium carbonate; 1,1'-binaphthyl-2,2'-diol in dimethyl sulfoxide T=50°C; 4 h;
参考文献
Tanimori, Shinji; Inaba, Ushio; Kato, Yoshihiro; Ura, Haruna; Kashiwagi, Hiroaki; Nishimura, Takeshi; Kirihata, Mitsunori
Research on Chemical Intermediates, 2014 , vol. 40, # 6 p. 2157 - 2164
615-43-0
2-碘苯胺
+
51721-68-7
4-甲氧基苄脒盐酸盐
→
反应条件
2620-81-7
2-(4-甲氧基苯基)-1H-苯并咪唑
反应条件
copper(I) oxide; caesium carbonate; N-methyl-2-(methylamino)ethylamine in N,N-dimethyl-formamide T=140°C; 16 h; Inert atmosphere;
参考文献
Qu, Yanyang; Pan, Lei; Wu, Zhiqing; Zhou, Xiangge
Tetrahedron, 2013 , vol. 69, # 6 p. 1717 - 1719
615-43-0
2-碘苯胺
+
874-90-8
4-甲氧基苯甲腈
→
反应条件
2620-81-7
2-(4-甲氧基苯基)-1H-苯并咪唑
反应条件
potassium tert-butylate in N,N-dimethyl acetamide T=80°C; 24 h; Schlenk techniqueInert atmosphere;
参考文献
Xiang, Shi-Kai; Tan, Wen; Zhang, Dong-Xue; Tian, Xian-Li; Feng, Chun; Wang, Bi-Qin; Zhao, Ke-Qing; Hu, Ping; Yang, Hua
Organic and Biomolecular Chemistry, 2013 , vol. 11, # 42 p. 7271 - 7275
615-43-0
2-碘苯胺
+
123-11-5
大茴香醛
→
反应条件
2620-81-7
2-(4-甲氧基苯基)-1H-苯并咪唑
反应条件
sodium azide; N,N,N',N,-tetramethylethylenediamine; copper(l) chloride in dimethyl sulfoxide T=120°C; 12 h;
参考文献
Kim, Yong; Kumar, Manian Rajesh; Park, Namjin; Heo, Yumi; Lee, Sunwoo
Journal of Organic Chemistry, 2011 , vol. 76, # 23 p. 9577 - 9583
3424-93-9
4-甲氧基苯甲酰胺
+
615-43-0
2-碘苯胺
→
反应条件
2620-81-7
2-(4-甲氧基苯基)-1H-苯并咪唑
反应条件
1: With copper(l) iodide; K3PO4*3H2O; N-methyl-2-(methylamino)ethylamine in 1,4-dioxane T=100°C; 3 h; Schlenk techniqueSealed tubeInert atmosphere; 2: With acetic acid in 1,4-dioxane Inert atmosphereSchlenk techniqueSealed tube;
参考文献
Yuan, Hua; Chen, Yongxin; Song, Jinli; Chen, Chunxia; Chen, Baohua
Chinese Journal of Chemistry, 2013 , vol. 31, # 10 p. 1247 - 1249
615-43-0
2-碘苯胺
→
反应条件
2525-35-1
3-乙基-1-甲基-1,3-二氢-2H-吲哚-2-酮
反应条件
2: NaH / dimethylsulfoxide 3: 23 percent / n-Bu3SnH, AIBN / toluene / 24 h / Heating View Scheme
参考文献
Bowman, W. Russell; Heaney, Harry; Jordan, Benjamin M.
Tetrahedron Letters, 1988 , vol. 29, # 50 p. 6657 - 6660
615-43-0
2-碘苯胺
→
反应条件
254114-34-6
反应条件
1.1: copper(l) iodide; bis-triphenylphosphine-palladium(II) chloride; diethylamine / 1 h / 40 °C / Inert atmosphere 2.1: triethylamine / dichloromethane / 2 h / 20 °C / Cooling with ice 3.1: sodium hydride / tetrahydrofuran; mineral oil / 0.5 h / Cooling with ice 3.2: 2 h / 20 °C 4.1: tris(dibenzylideneacetone)dipalladium(0) chloroform complex; tris-(o-tolyl)phosphine / tetrahydrofuran; hexane / 0.67 h / 20 - 60 °C / Inert atmosphere 5.1: (1S)-10-camphorsulfonic acid / methanol; dichloromethane / 24 h / 20 °C / Inert atmosphere 6.1: (CuOTf)2*C6H5CH3 / acetonitrile / 1 h / 20 °C 7.1: pyridinium chlorochromate / dichloromethane / 3 h / 20 °C 8.1: diphenyl diselenide; dihydrogen peroxide / dichloromethane / 24 h / 20 °C / Inert atmosphere 8.2: 16 h 9.1: diphenyl diselenide; dihydrogen peroxide / dichloromethane / 48 h / 20 °C / Inert atmosphere 9.2: 16 h 10.1: palladium 10 on activated carbon; hydrogen / ethyl acetate / 1 h / 20 °C / 760.05 Torr View Scheme
参考文献
Bhosale, Shrikar M.; Gawade, Rupesh L.; Puranik, Vedavati G.; Kusurkar, Radhika S.
Tetrahedron Letters, 2012 , vol. 53, # 23 p. 2894 - 2896
3731-52-0
+
615-43-0
2-碘苯胺
→
反应条件
2612-72-8
反应条件
1,4-diaza-bicyclo[2.2.2]octane; 1,10-phenanthroline; copper (II) acetate monohydrate; sulfur in dimethyl sulfoxide T=100°C;
参考文献
Wang, Rui; Ding, Yong-Liang; Liu, Hong; Peng, Shu; Ren, Jie; Li, Lei
Tetrahedron Letters, 2014 , vol. 55, # 4 p. 945 - 949
119-61-9
+
615-43-0
2-碘苯胺
→
反应条件
2720-93-6
反应条件
1: toluene-4-sulfonic acid / toluene / |Molecular sieve; |Inert atmosphere; |Dean-Stark; |Reflux 2: palladium diacetate; triphenylphosphine; silver carbonate / 1,4-dioxane / 10 h / 120 °C / |Sealed tube View Scheme
参考文献
Mahajan, Jyoti P.; Suryawanshi, Yogeshwar R.; Mhaske, Santosh B.
Organic Letters, 2012 , vol. 14, # 22 p. 5804 - 5807
615-43-0
2-碘苯胺
→
反应条件
26216-91-1
反应条件
1.1: bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; diethylamine / N,N-dimethyl acetamide / 1 h / 20 °C 1.2: 140 °C 2.1: sodium cyanoborohydride / acetic acid / 20 h / 20 °C View Scheme
参考文献
Yu, Xufen; Park, Eun-Jung; Kondratyuk, Tamara P.; Pezzuto, John M.; Sun, Dianqing
Organic and Biomolecular Chemistry, 2012 , vol. 10, # 44 p. 8835 - 8847
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