对称-DI-O-苯甲基脲合成路线 (共 67 条)
反应条件
tin(IV) chloride; triethylamine; [Pt(triphenylphosphine)2Cl2] in benzene
T=140°C; 4 h;
参考文献
Tsuji, Yasushi; Takeuchi, Ryo; Watanabe, Yoshihisa
Journal of Organometallic Chemistry, 1985 , vol. 290, p. 249 - 256
反应条件
sodium periodate; ammonia in water; N,N-dimethyl-formamide
T=80 - 85°C; 0.5 h;
参考文献
Ramadas; Janarthanan; Pritha
Synlett, 1997 , vol. 1997, # 9 p. 1053 - 1054
反应条件
sodium chlorite
0.5 h; Heatingfurther reagents;
参考文献
Ramadas; Janarthanan
Synthetic Communications, 1997 , vol. 27, # 13 p. 2357 - 2362
反应条件
sodium azide; [bis(acetoxy)iodo]benzene in acetonitrile
T=0 - 80°C; 36 h; Inert atmosphere;
参考文献
Li, Xiao-Qiang; Wang, Wei-Kun; Han, Yi-Xin; Zhang, Chi
Advanced Synthesis and Catalysis, 2010 , vol. 352, # 14-15 p. 2588 - 2598
反应条件
KO2 in tetrahydrofuran
T=20°C; 35 h;
参考文献
Kim,Yong Hae; Yon, Gyu Hwan
Journal of the Chemical Society, Chemical Communications, 1983 , # 13 p. 715 - 716
反应条件
1: 1-tert-butyl-1-isopropyl-3-phenylurea With n-butyllithium; N,N,N',N,-tetramethylethylenediamine in diethyl ether; hexane
T=0°C; 3 h; Inert atmosphere;
2: methyl iodide With water in diethyl ether; hexane
T=0°C; Inert atmosphere;
参考文献
Houlden, Chris E.; Lloyd-Jones, Guy C.; Booker-Milburn, Kevin I.
Organic Letters, 2010 , vol. 12, # 13 p. 3090 - 3092
反应条件
dichlorotris(triphenylphosphine)ruthenium(II) in 1,3,5-trimethyl-benzene
12 h; Heating;
参考文献
Kotachi, Shinji; Tsuji, Yasushi; Kondo, Teruyuki; Watanabe, Yoshihisa
Journal of the Chemical Society, Chemical Communications, 1990 , # 7 p. 549 - 550
反应条件
carbon monoxide; benzene; dodecacarbonyltetrarhodium(0)
T=220°C; 6 h;
参考文献
Mise, Takaya; Hong, Pangbu; Yamazaki, Hiroshi
Chemistry Letters, 1980 , p. 439 - 440
反应条件
benzene; dodecacarbonyltetrarhodium(0)
T=220°C; 6 h;
参考文献
Mise, Takaya; Hong, Pangbu; Yamazaki, Hiroshi
Chemistry Letters, 1980 , p. 439 - 440
反应条件
selenium; oxygen; triethylamine in toluene
T=140°C; 3 h; Autoclave;
参考文献
Zhang, Xiaopeng; Li, Desheng; Ma, Xueji; Wang, Yan; Zhang, Guisheng
Synthesis (Germany), 2013 , vol. 45, # 10 art. no. SS-2013-F0083-OP, p. 1357 - 1363