(2E,4E)-5-(6-甲氧基-1,3-苯并二氧戊环-5-基)-1-哌啶-1-基戊-2,4-二烯-1-酮合成路线 （共 5 条）
反应条件
1: 70 percent / phosphorus oxychloride / 2.5 h / Heating
2: 60 percent / zinc, iodine / tetrahydrofuran / 2 h / Heating
3: 44 percent / 2N methanolic KOH / 3 h / Heating
4: oxalyl chloride / benzene / 2 h / Heating
5: benzene / Ambient temperature
View Scheme
参考文献
Okwute, S. K.; Okogun, J. I.; Okorie, D. A.
Tetrahedron, 1984 , vol. 40, # 13 p. 2541 - 2546
反应条件
1: 60 percent / zinc, iodine / tetrahydrofuran / 2 h / Heating
2: 44 percent / 2N methanolic KOH / 3 h / Heating
3: oxalyl chloride / benzene / 2 h / Heating
4: benzene / Ambient temperature
View Scheme
参考文献
Okwute, S. K.; Okogun, J. I.; Okorie, D. A.
Tetrahedron, 1984 , vol. 40, # 13 p. 2541 - 2546
反应条件
1: oxalyl chloride / benzene / 2 h / Heating
2: benzene / Ambient temperature
View Scheme
参考文献
Okwute, S. K.; Okogun, J. I.; Okorie, D. A.
Tetrahedron, 1984 , vol. 40, # 13 p. 2541 - 2546
反应条件
1: 44 percent / 2N methanolic KOH / 3 h / Heating
2: oxalyl chloride / benzene / 2 h / Heating
3: benzene / Ambient temperature
View Scheme
参考文献
Okwute, S. K.; Okogun, J. I.; Okorie, D. A.
Tetrahedron, 1984 , vol. 40, # 13 p. 2541 - 2546
反应条件
in benzene
Ambient temperature; Yield given;
参考文献
Okwute, S. K.; Okogun, J. I.; Okorie, D. A.
Tetrahedron, 1984 , vol. 40, # 13 p. 2541 - 2546
