acetic acid in ethanol
T=160°C; 0.166667 h; microwave irradiation;
参考文献
Zhao, Zhijian; Robinson, Ronald G.; Barnett, Stanley F.; Defeo-Jones, Deborah; Jones, Raymond E.; Hartman, George D.; Huber, Hans E.; Duggan, Mark E.; Lindsley, Craig W.
Bioorganic and Medicinal Chemistry Letters, 2008 , vol. 18, # 1 p. 49 - 53
1: 1,2-diaminobenzene-4-carboxylic acid; 1-(4-{[4-(2-oxo-2,3-dihydro-1H-benzimidazol-1-yl)piperidin-1-yl]methyl}phenyl)-2-phenylethane-1,2-dione With acetic acid in ethanol
T=160°C; 0.166667 h; microwave irradiation;
2: 1-amino-2-diethylamino-ethane With PS-DCC; benzotriazol-1-ol; N-ethyl-N,N-diisopropylamine in dichloromethane
Further stages.;
参考文献
Zhao, Zhijian; Robinson, Ronald G.; Barnett, Stanley F.; Defeo-Jones, Deborah; Jones, Raymond E.; Hartman, George D.; Huber, Hans E.; Duggan, Mark E.; Lindsley, Craig W.
Bioorganic and Medicinal Chemistry Letters, 2008 , vol. 18, # 1 p. 49 - 53
UNIVERSITY OF SUNDERLAND; TODD, Adam; ANDERSON, Rosaleen Joy; SMALL, David Antony Philip; GROUNDWATER, Paul William; BENTON, Matthew Richard
Patent: WO2014/96864 A1, 2014 ;