反应条件
1: phenyllithium With 3-butyl-1,1-dimethyl-1,3-dihydro-benzo[c][1,2]oxasilole in tetrahydrofuran; anhydrous butyl ether T=-78 - 20°C; 1 h; Inert atmosphere; 2: 4-iodo-benzoic acid methyl ester With copper(l) iodide; dpca; palladium dichloride in tetrahydrofuran; anhydrous butyl ether T=20°C; 2 h; Inert atmosphere;
参考文献
THE TRUSTEES OF THE UNIVERSITY OF PENNSYLVANIA; HOYE, Adam, T.; KIM, Won-suk; MARTINEZ-SOLORIO, Dionicio; SMITH, Amos, B.; SANCHEZ, Luis; TONG, Rongbiao; NGUYEN, Minh, Huu
Patent: WO2013/185021 A2, 2013 ;
Location in patent: Paragraph 0049 ;
