4,4'-二甲基二苯胺合成路线 （共 114 条）
反应条件
1: With nitric acid; acetic acid
0.166667 h; Cooling with ice;
2: With isopentyl nitrite
0.116667 h; Cooling with ice; regioselective reaction;
参考文献
Munha, Rui F.; Zarkesh, Ryan A.; Heyduk, Alan F.
Inorganic Chemistry, 2013 , vol. 52, # 19 p. 11244 - 11255
反应条件
n-Pentyl nitrite; nitric acid
参考文献
Krollpfeiffer; Wolf; Walbrecht
Chemische Berichte, 1934 , vol. 67, p. 908,914
参考文献
Krollpfeiffer; Wolf; Walbrecht
Chemische Berichte, 1934 , vol. 67, p. 908,914
反应条件
1: pyrene; 1,3-dibromo-5,5-dimethyl-hydantoin in dichloromethane
T=20°C; 1 h;
2: 4,4'-dimethyldiphenylamine With tri-tert-butyl phosphine; palladium diacetate; caesium carbonate in o-xylene
T=120°C; Buchwald-Hartwig Coupling; 48 h; Overall yield = 73 percent;
参考文献
Hu, Jian-Yong; Feng, Xing; Seto, Nobuyuki; Do, Jung-Hee; Zeng, Xi; Tao, Zhu; Yamato, Takehiko
Journal of Molecular Structure, 2013 , vol. 1035, p. 19 - 26
反应条件
triethylamine; trichloromethyl chloroformate in dichloromethane
T=20°C; 1 h;
参考文献
Han, Ki-Jong; Tae, Beom Seok; Kim, Misoo
Organic Preparations and Procedures International, 2005 , vol. 37, # 2 p. 198 - 203
参考文献
Hellwinkel, Dieter; Laemmerzahl, Frank; Hofmann, Gunter
Chemische Berichte, 1983 , vol. 116, # 10 p. 3375 - 3405
参考文献
Hellwinkel, Dieter; Laemmerzahl, Frank; Hofmann, Gunter
Chemische Berichte, 1983 , vol. 116, # 10 p. 3375 - 3405
参考文献
Hellwinkel, Dieter; Laemmerzahl, Frank; Hofmann, Gunter
Chemische Berichte, 1983 , vol. 116, # 10 p. 3375 - 3405
参考文献
Budyka, M. F.; Laukhina, O. D.; Sazhnikov, V. A.; Stunzhas, M. G.; Alfimov, M. V.
Doklady Chemistry, 1989 , vol. 309, # 4-6 p. 351 - 353
Dokl. Akad. Nauk SSSR Ser. Khim., 1989 , vol. 309, # 5 p. 1126 - 1129
反应条件
in hexane
Irradiation;
参考文献
Budyka, M. F.; Laukhina, O. D.; Sazhnikov, V. A.; Stunzhas, M. G.; Alfimov, M. V.
Doklady Chemistry, 1989 , vol. 309, # 4-6 p. 351 - 353
Dokl. Akad. Nauk SSSR Ser. Khim., 1989 , vol. 309, # 5 p. 1126 - 1129
