4,4’-二甲基二苯硫醚合成路线 （共 108 条）
反应条件
sulenium monochloride
1.) ether, -40 deg C, 2 h, 2.) ether, 3 h; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Bertini, Vincenzo; Munno, Angela De; Picci, Nevio; Lucchesini, Francesco; Pocci, Marco
Heterocycles, 1987 , vol. 26, # 8 p. 2153 - 2158
反应条件
sulenium monochloride
1.) ether, -40 deg C, 2 h, 2.) ether, 3 h; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Bertini, Vincenzo; Munno, Angela De; Picci, Nevio; Lucchesini, Francesco; Pocci, Marco
Heterocycles, 1987 , vol. 26, # 8 p. 2153 - 2158
反应条件
in benzene
0.5 h; Heating; Product distribution; Further Variations:molar ratios;
参考文献
Nakayama, Juzo; Tai, Ayako; Iwasa, Sachiko; Furuya, Tomohiro; Sugihara, Yoshiaki
Tetrahedron Letters, 2005 , vol. 46, # 9 p. 1395 - 1397
反应条件
Destillation des Reaktionsprodukts mit Wasserdampf;
参考文献
Gilman; Smith; Parker
Journal of the American Chemical Society, 1925 , vol. 47, p. 858
反应条件
in methanol; benzene
T=20°C; Rate constant;
参考文献
Demarcq, Michel C.
Journal of Chemical Research, Miniprint, 1993 , # 11 p. 3052 - 3080
反应条件
Abdestillieren des Reaktionsgemisches mit Wasserdampf;
参考文献
Gilman; Smith; Parker
Journal of the American Chemical Society, 1925 , vol. 47, p. 858
反应条件
aluminium trichloride
T=25°C; Disproportionation; substitution; 0.5 h; Product distribution; Further Variations:time;
参考文献
Takeuchi, Hiroshi; Suga, Keisuke
Journal of the Chemical Society. Perkin Transactions 2, 2000 , # 9 p. 1803 - 1808
反应条件
T=200°C; 10 h; Product distributionMechanism;
参考文献
El-Khawaga, A. M.; El-Zohry, M. F.; Ismail, M. T.; Abdel-Wahab, A. M.
Phosphorus and Sulfur and the Related Elements, 1987 , vol. 34, p. 63 - 68
反应条件
T=220 - 250°C; im Rohr und anschliessend Destillieren im Vakuum;
参考文献
Rosenmund; Harms
Chemische Berichte, 1920 , vol. 53, p. 2238
反应条件
T=25°C; Extraktion des (mit verd.Schwefelsaeure zersetzten) Reaktionsprodukts mit verd.Alkali;
参考文献
Miller; Smiles
Journal of the Chemical Society, 1925 , vol. 127, p. 231
