4,4’-二甲基二苯硫醚合成路线 (共 108 条)
反应条件
silver carbonate; palladium dichloride in 1,2-dichloro-ethane
T=120°C; 0.166667 h; Microwave irradiation;
参考文献
Li, Junchen; Bi, Xiaojing; Wang, Hongmei; Xiao, Junhua
RSC Advances, 2014 , vol. 4, # 37 p. 19214 - 19217
反应条件
aluminium trichloride
参考文献
Deuss
Recueil des Travaux Chimiques des Pays-Bas, 1909 , vol. 28, p. 136
反应条件
hydrogen sulfide; sulfur
T=184°C; 15 h;
参考文献
Papernaya, L. K.; Panova, G. M.; Deryagina, E. N.; Voronkov, M. G.
Russian Journal of Organic Chemistry, 1993 , vol. 29, # 11.2 p. 1856 - 1862
Zhurnal Organicheskoi Khimii, 1993 , vol. 29, # 11 p. 2238 - 2245
反应条件
tetrakis(triphenylphosphine) palladium(0); potassium carbonate in tetrahydrofuran
Suzuki-Miyaura cross-coupling; Heating; Product distribution; Further Variations:Reagents;
参考文献
Dubbaka, Srinivas Reddy; Vogel, Pierre
Organic Letters, 2004 , vol. 6, # 1 p. 95 - 98
反应条件
copper(l) iodide; 1,10-phenanthroline in dimethylsulfoxide-d6
T=110°C; 24 h; Inert atmosphere; ConcentrationReagent/catalyst;
参考文献
Chen, Chaohuang; Weng, Zhiqiang; Hartwig, John F.
Organometallics, 2012 , vol. 31, # 22 p. 8031 - 8037
反应条件
1: 1-(iodo)-4-methylbenzene With potassium tert-butylate; thiolacetic acid potassium salt in dimethyl sulfoxide
3 h; Irradiation;
2: methyl iodide in water; dimethyl sulfoxide
参考文献
Schmidt, Luciana C.; Rey, Valentina; Penenory, Alicia B.
European Journal of Organic Chemistry, 2006 , # 9 p. 2210 - 2214
反应条件
hydrogen iodide
T=100°C; im Einschlussrohr;
参考文献
Fischer,E.
Chemische Berichte, 1915 , vol. 48, p. 97
反应条件
in dimethylsulfoxide-d6
T=110°C; 3 h; Inert atmosphere;
参考文献
Chen, Chaohuang; Weng, Zhiqiang; Hartwig, John F.
Organometallics, 2012 , vol. 31, # 22 p. 8031 - 8037
反应条件
in dimethylsulfoxide-d6
T=110°C; 6 h; Inert atmosphere;
参考文献
Chen, Chaohuang; Weng, Zhiqiang; Hartwig, John F.
Organometallics, 2012 , vol. 31, # 22 p. 8031 - 8037
反应条件
in hexadeuterioacetone
T=20°C; Inert atmosphereIrradiation; Thermodynamic data;
参考文献
Kampmeier, Jack A.; Mansurul Hoque; Saeva, Franklin D.; Wedegaertner, Donald K.; Thomsen, Pia; Ullah, Saif; Krake, Jacob; Lund, Torben
Journal of the American Chemical Society, 2009 , vol. 131, # 29 p. 10015 - 10022